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MassMS-NW-1299 2,2-dimethyl-1,3-dioxolane-4-methanol C6H12O3 (Mass of molecular ion: 132)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 9.4 19.0 1.4 27.0 5.5 28.0 2.0 29.0 6.6 31.0 11.5 39.0 4.6 40.0 1.3 41.0 10.7 42.0 10.9 43.0 100.0 44.0 4.0 45.0 2.0 55.0 1.6 57.0 27.6 58.0 3.2 59.0 21.2 60.0 1.0 61.0 16.3 72.0 11.9 73.0 5.7 75.0 1.3 83.0 2.0 101.0 30.3 102.0 1.7 117.0 41.8 118.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 O3 0.04 ml : 0.5 ml CDCl3 2,2-dimethyl-1,3-dioxolane-4-methanol 
Assign. Shift(ppm)
A 4.25 B *1 4.04 C *1 3.77 D *2 3.710 E *2 3.624 F 2.59 G *3 1.44 J *3 1.38
Hz ppm Int.386.06 4.311 36 384.75 4.297 56 382.19 4.268 37 380.88 4.253 64 379.75 4.241 81 378.31 4.225 50 376.00 4.199 67 374.56 4.183 60 373.38 4.170 69 369.13 4.122 175 362.88 4.052 55 361.25 4.034 275 355.00 3.964 170 344.75 3.850 255 342.25 3.822 51 338.44 3.779 230 336.94 3.763 152 330.69 3.693 344 327.75 3.660 273 326.88 3.650 250 322.88 3.606 172 316.19 3.531 36 311.19 3.475 31 232.25 2.594 216 129.38 1.445 919 128.88 1.440 967 123.31 1.377 1000 122.75 1.371 846
CCl4 solution
liquid film
4880 A,200 M,liquid
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