TRANS-TRIPHENYL(1-PROPENYL)PHOSPHONIUMCHLORIDE
Product Name TRANS-TRIPHENYL(1-PROPENYL)PHOSPHONIUMCHLORIDE
MFC21H20ClP
MW338.810261
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MassMS-NW-7019 trans-triphenyl(1-propenyl)phosphonium chloride C21H20ClP (Mass of molecular ion: 338)
Source Temperature: 240 °C Sample Temperature: 140 °C Direct, 75 eV
27.0 1.9 35.0 1.4 36.0 3.4 38.0 1.1 39.0 5.3 41.0 1.1 50.0 4.3 51.0 14.0 52.0 1.8 56.0 1.1 57.0 4.0 63.0 3.0 65.0 3.5 69.0 1.2 74.0 1.2 75.0 1.5 76.0 1.6 77.0 7.9 78.0 3.8 79.0 1.4 80.0 1.6 81.0 3.8 82.0 1.3 83.0 2.0 89.0 1.7 91.0 5.2 102.0 1.5 105.0 1.1 107.0 18.3 108.0 27.8 109.0 3.7 115.0 7.4 116.0 1.8 117.0 1.5 120.0 1.1 121.0 1.3 126.0 1.0 128.0 2.7 129.0 1.1 131.0 2.0 133.0 5.0 139.0 2.9 141.0 2.8 151.0 1.4 152.0 10.9 153.0 3.1 154.0 3.1 157.0 6.0 165.0 1.5 170.0 3.7 181.0 2.0 182.0 1.2 183.0 76.4 184.0 15.8 185.0 12.1 186.0 2.3 259.0 1.3 260.0 1.4 261.0 16.2 262.0 100.0 263.0 20.6 264.0 2.3 275.0 11.0 276.0 4.5 277.0 2.1 301.0 3.5 302.0 3.4 303.0 1.6 328.0 1.4 342.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C21 H20 Cl P 0.036 g : 0.5 ml CDCl3 trans-triphenyl(1-propenyl)phosphonium chloride 
Assign. Shift(ppm)
A 7.850 B 7.746 C 7.686 D 7.66 E 6.646 F 2.354 J(A,P-31)=2.0HZ J(B,P-31)=3.8HZ J(C,P-31)12.9HZ J(E,F)=6.8HZ J(D,E)=16.7HZ J(E,P-31)=22HZ J(D,P-31)=22HZ
Hz ppm Int.3154.91 7.895 30 3152.22 7.888 40 3150.27 7.883 51 3149.78 7.882 51 3147.58 7.876 120 3146.12 7.873 216 3144.41 7.868 242 3143.07 7.865 165 3140.99 7.860 173 3138.92 7.855 506 3136.84 7.849 563 3135.01 7.845 208 3133.06 7.840 236 3131.47 7.836 381 3130.74 7.834 327 3129.39 7.831 389 3128.17 7.828 217 3124.27 7.818 56 3123.05 7.815 49 3122.44 7.813 47 3121.46 7.811 46 3120.61 7.809 46 3119.26 7.805 53 3118.53 7.804 54 3117.80 7.802 56 3117.43 7.801 56 3116.94 7.800 58 3115.84 7.797 63 3105.96 7.772 444 3104.13 7.768 314 3102.17 7.763 524 3100.59 7.759 367 3099.37 7.756 464 3097.90 7.752 912 3095.58 7.746 544 3094.12 7.743 937 3090.33 7.733 683 3086.67 7.724 636 3084.59 7.719 293 3083.37 7.716 310 3081.79 7.712 827 3080.69 7.709 1000 3075.56 7.696 235 3073.61 7.691 570 3072.02 7.687 474 3067.75 7.677 992 3062.38 7.663 301 3060.55 7.659 675 3059.20 7.655 505 3052.12 7.637 34 3051.51 7.636 32 2677.61 6.700 90 2670.90 6.684 94 2667.60 6.675 31 2664.31 6.667 35 2662.11 6.662 47 2661.01 6.659 93 2655.64 6.645 107 2654.42 6.642 104 2649.05 6.629 98 2645.75 6.621 32 2642.33 6.612 32 2639.16 6.604 84 2632.45 6.587 83 952.88 2.385 31 952.51 2.384 31 946.29 2.368 382 944.58 2.364 489 943.97 2.362 508 942.26 2.358 424 939.58 2.352 405 937.87 2.347 492 937.38 2.346 499 935.67 2.342 396 931.27 2.331 37
in CDCl3
KBr disc
nujol mull
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