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N,N-Dimethyl-p-toluidine

Product Name N,N-Dimethyl-p-toluidine

CAS99-97-8

MFC9H13N

MW135.21

¹³CNMR

Mass

MS-NW-0584          
N,N-dimethyl-p-toluidine
C9H13N              (Mass of molecular ion:    135)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       2.0
      27.0       1.4
      39.0       4.5
      41.0       1.8
      42.0       4.6
      44.0       1.7
      50.0       1.5
      51.0       3.4
      52.0       1.6
      63.0       2.7
      65.0       7.5
      66.0       1.1
      66.5       3.0
      67.0       1.0
      67.5       2.5
      77.0       4.6
      78.0       1.9
      79.0       1.3
      89.0       1.9
      90.0       1.5
      91.0      17.8
      92.0       3.3
      93.0       1.5
     104.0       1.0
     105.0       1.6
     106.0       1.0
     117.0       1.1
     118.0      11.2
     119.0      13.2
     120.0       6.4
     121.0       1.3
     132.0       1.4
     133.0       1.3
     134.0     100.0
     135.0      76.2
     136.0       7.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
N,N-dimethyl-p-toluidine

    Assign.     Shift(ppm)

      A             7.02
      B             6.665
      C             2.856
      D             2.238

     Hz     ppm     Int.

    634.69   7.087     65
    634.00   7.080     60
    633.25   7.071     37
    632.44   7.062     28
    631.75   7.054     24
    628.13   7.014     35
    627.50   7.007     38
    626.44   6.995     60
    625.81   6.988     96
    625.19   6.981     84
    602.88   6.732     21
    600.25   6.703    115
    598.00   6.678     36
    593.69   6.629     31
    591.50   6.605     68
    255.88   2.858   1000
    200.50   2.239    280

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

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