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MS-NW-0437 (1,2-epoxyethyl)benzene C8H8O (Mass of molecular ion: 120)
Source Temperature: 240 °C Sample Temperature: 120 °C Reservoir, 75 eV
27.0 1.3 29.0 1.3 37.0 1.0 38.0 2.6 39.0 10.7 40.0 1.3 41.0 1.9 43.0 1.6 50.0 4.8 51.0 8.8 52.0 1.7 61.0 1.3 62.0 3.4 63.0 9.7 64.0 3.9 65.0 15.0 66.0 1.0 74.0 1.6 75.0 1.0 77.0 4.0 78.0 1.3 89.0 26.8 90.0 34.7 91.0 100.0 92.0 29.8 93.0 2.0 104.0 1.5 105.0 1.7 119.0 21.2 120.0 35.9 121.0 3.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H8 O 0.05 ml : 0.5 ml CDCl3 (1,2-epoxyethyl)benzene Assign. Shift(ppm)
A 7.28 B 3.817 C 3.091 D 2.758 J(B,C)=4.1HZ J(B,D)=2.6HZ J(C,D)=5.5HZ
Hz ppm Int.
661.06 7.382 29 659.63 7.366 36 654.50 7.308 251 652.38 7.285 1000 648.25 7.239 109 645.75 7.211 60 645.00 7.202 78 643.13 7.181 53 345.31 3.856 99 342.75 3.828 115 341.25 3.811 117 338.69 3.782 109 282.06 3.150 103 277.94 3.104 107 276.50 3.088 147 272.44 3.042 127 250.56 2.798 149 248.00 2.770 143 245.06 2.737 108 242.50 2.708 98
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