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MassMS-NW-1086 phenylhydrazine C6H8N2 (Mass of molecular ion: 108)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
16.0 2.2 17.0 3.0 18.0 6.2 26.0 2.0 27.0 5.5 28.0 18.1 29.0 4.7 30.0 1.3 31.0 2.6 37.0 5.0 38.0 8.5 39.0 22.7 40.0 3.3 41.0 5.2 46.5 1.0 49.0 2.2 50.0 17.5 51.0 40.6 52.0 14.3 53.0 3.7 54.0 4.0 61.0 2.0 62.0 2.9 63.0 8.8 64.0 9.7 65.0 46.4 66.0 12.7 67.0 1.7 69.0 2.8 73.0 1.6 74.0 5.2 75.0 2.9 76.0 3.7 77.0 84.3 78.0 47.1 79.0 12.2 80.0 4.5 81.0 1.6 87.0 1.2 90.0 1.0 91.0 16.8 92.0 44.0 93.0 35.0 94.0 2.5 105.0 10.6 106.0 29.5 107.0 6.9 108.0 100.0 109.0 7.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H8 N2 0.04 ml : 0.5 ml CDCl3 phenylhydrazine 
Assign. Shift(ppm)
A 7.21 B 6.80 C 6.76 D 4.0
Hz ppm Int.655.13 7.315 259 654.31 7.306 322 652.44 7.285 198 649.50 7.253 93 648.69 7.244 212 647.94 7.235 411 647.44 7.230 276 646.88 7.223 452 646.06 7.214 514 645.13 7.204 383 644.06 7.192 111 641.81 7.167 208 639.75 7.144 361 639.25 7.138 546 638.56 7.130 603 636.69 7.110 140 617.00 6.890 133 616.00 6.879 214 615.50 6.873 284 614.50 6.862 429 611.75 6.831 230 610.13 6.813 744 609.50 6.806 1000 609.13 6.802 978 607.44 6.783 837 603.63 6.740 250 603.13 6.735 238 602.38 6.726 223 601.81 6.720 605 601.06 6.712 799 600.56 6.706 596 599.81 6.698 136 598.06 6.678 76 358.00 3.998 175
in CDCl3
CCl4 solution
liquid film
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