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MassMS-NW-0050 indene C9H8 (Mass of molecular ion: 116)
Source Temperature: 210 °C Sample Temperature: 55 °C Reservoir, 75 eV
38.0 1.5 39.0 5.6 50.0 3.2 51.0 3.1 57.0 1.0 57.5 3.0 58.0 2.6 61.0 1.4 62.0 4.1 63.0 9.8 64.0 1.3 65.0 3.0 74.0 1.9 75.0 1.6 86.0 1.6 87.0 2.2 88.0 1.8 89.0 10.1 90.0 1.2 103.0 1.5 113.0 2.2 114.0 2.9 115.0 79.3 116.0 100.0 117.0 12.4 118.0 2.7 119.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H8 22.1 mg : 0.5 ml CDCl3 indene 
Assign. Shift(ppm)
A 7.466 B 7.400 C 7.263 D 7.187 E 6.879 F 6.547 G 3.385 C WAS DECOUPLED BY IRRADIATION AT G. J(E,F)=5.5HZ. J(F,G)=1.9HZ. J(E,G)=2.0HZ. J(A,E)=0.7HZ.
Hz ppm Int.2990.60 7.484 63 2989.87 7.482 172 2989.01 7.480 285 2988.65 7.479 255 2987.79 7.477 284 2987.06 7.475 178 2986.21 7.473 72 2984.99 7.470 34 2983.28 7.465 83 2982.42 7.463 209 2981.69 7.461 324 2980.83 7.459 297 2980.47 7.458 328 2979.61 7.456 209 2978.88 7.454 87 2962.65 7.414 222 2961.67 7.411 298 2960.82 7.409 222 2958.74 7.404 31 2957.52 7.401 33 2955.20 7.395 294 2954.22 7.393 403 2953.37 7.390 282 2950.56 7.383 31 2911.74 7.286 98 2911.13 7.285 180 2910.52 7.283 177 2909.91 7.282 179 2909.30 7.280 95 2904.30 7.268 223 2903.69 7.266 395 2903.08 7.265 378 2902.47 7.263 370 2901.86 7.262 192 2900.39 7.258 34 2899.78 7.256 32 2898.80 7.254 31 2898.19 7.252 31 2896.85 7.249 133 2896.24 7.247 232 2895.63 7.246 220 2895.02 7.244 213 2894.41 7.243 112 2881.71 7.211 31 2880.86 7.209 31 2879.03 7.204 276 2878.66 7.203 312 2878.30 7.203 320 2877.81 7.201 287 2877.44 7.200 256 2874.88 7.194 30 2874.27 7.192 33 2873.54 7.191 37 2871.70 7.186 379 2871.22 7.185 372 2870.48 7.183 382 2867.68 7.176 32 2866.21 7.172 30 2864.26 7.167 157 2863.89 7.166 157 2863.04 7.164 155 2862.67 7.163 143 2754.64 6.893 135 2753.91 6.891 144 2752.69 6.888 282 2751.95 6.886 267 2750.73 6.883 166 2749.88 6.881 168 2749.15 6.879 171 2748.29 6.877 176 2747.19 6.874 309 2746.34 6.872 299 2745.12 6.869 174 2744.38 6.867 157 2621.22 6.559 185 2619.26 6.554 369 2617.31 6.550 209 2615.72 6.546 189 2613.77 6.541 342 2611.69 6.535 183 1355.10 3.391 545 1353.76 3.388 731 1353.15 3.386 1000 1352.42 3.385 701 1351.20 3.381 560 1350.46 3.380 369 1346.44 3.370 42
in CDCl3
CCl4 solution
liquid film
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