SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List >  920-46-7More Spectrum > Methacryloyl chloride (920-46-7)MS

920-46-7

Methacryloyl chloride

Product Name Methacryloyl chloride

CAS920-46-7

MFC4H5ClO

MW104.53

More

  • 920-46-7_ms
    Mass

    MS-IW-3680          
    methacryloyl chloride
    C4H5ClO             (Mass of molecular ion:    104)
    

       Source Temperature: 210 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          15.0       1.3
          25.0       1.4
          26.0       3.9
          27.0       2.7
          28.0       3.2
          35.0       1.3
          36.0       2.9
          37.0       7.9
          38.0      11.6
          39.0      59.0
          40.0       9.1
          41.0      75.5
          42.0       3.4
          43.0       4.2
          49.0       1.7
          50.0       1.3
          51.0       1.2
          53.0       2.9
          55.0       1.0
          63.0       3.7
          65.0       1.1
          69.0     100.0
          70.0       6.0
          75.0       1.2
          76.0       8.6
          77.0       2.8
          78.0       3.0
          79.0       1.4
          81.0       3.1
          89.0       1.5
         105.0       1.9
         109.0       2.4
         145.0       8.0
         147.0       2.6
         208.0       2.5
         210.0       1.6
    

400 MHz in CDCl3

parameter in CCl4

  • 920-46-7_1hnmr_2

    1H NMR 399.65 MHz
    C4 H5 Cl O 0.05 ml : 0.5 ml CDCl3
    methacryloyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.509 B 6.058 C 2.019

         Hz     ppm     Int.
    

       2602.29   6.512    469
       2601.32   6.509    437
       2423.58   6.065    178
       2422.12   6.061    427
       2420.65   6.057    415
       2419.07   6.053    176
        808.35   2.023   1000
        807.50   2.021    926
        806.76   2.019    835
        805.91   2.017    781
    

  • 920-46-7_1hnmr

    1H NMR 300 MHz
    C4 H5 Cl O 5 % in CCl4
    methacryloyl chloride
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.02 D(B) 6.48 D(C) 2.03 J(A,B) 0.0 J(A,C) -1.5 J(B,C) -0.90 JACKMAN,L.M. & WILEY,R.H. J.CHEM.SOC. 1960, 2881

         Hz     ppm     Int.
    

       1944.43   6.481    404
       1943.60   6.479    404
       1808.27   6.028    136
       1806.77   6.023    357
       1805.27   6.018    358
       1803.78   6.013    136
        610.20   2.034    818
        609.24   2.031   1000
        608.78   2.029    999
        607.83   2.026    815
    

in CDCl3

  • 920-46-7_13cnmr

liquid film

  • 920-46-7_ir1