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MassMS-NW-6038 1-phenylpiperazine C10H14N2 (Mass of molecular ion: 162)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.2 27.0 2.1 28.0 5.7 29.0 5.2 30.0 3.7 39.0 1.9 41.0 1.4 42.0 3.0 50.0 1.5 51.0 5.6 52.0 1.0 56.0 8.8 57.0 4.8 65.0 1.3 77.0 12.3 78.0 2.1 79.0 1.3 81.0 1.7 91.0 5.3 93.0 1.0 100.0 1.2 104.0 9.5 105.0 11.6 106.0 7.1 107.0 1.6 118.0 1.3 120.0 100.0 121.0 9.3 132.0 1.3 162.0 32.6 163.0 4.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 N2 0.05 ml : 0.5 ml CDCl3 1-phenylpiperazine 
Assign. Shift(ppm)
A 7.237 B 6.889 C 6.834 D 3.072 E 2.949 F 2.44
Hz ppm Int.2900.15 7.257 518 2899.29 7.255 290 2898.07 7.252 209 2896.73 7.249 223 2895.26 7.245 128 2892.82 7.239 643 2891.36 7.235 692 2889.04 7.229 142 2886.11 7.222 215 2884.89 7.219 240 2884.03 7.217 594 2758.18 6.902 525 2757.08 6.899 688 2755.00 6.894 302 2750.37 6.882 332 2749.27 6.880 582 2748.29 6.877 582 2739.38 6.855 180 2738.28 6.852 286 2737.18 6.849 177 2731.93 6.836 241 2730.96 6.834 451 2730.10 6.832 266 2724.73 6.818 139 2723.75 6.816 231 2722.66 6.813 146 1233.64 3.087 750 1228.88 3.075 904 1226.56 3.070 628 1223.63 3.062 1000 1182.98 2.961 851 1180.05 2.953 536 1177.73 2.947 757 1172.97 2.935 605 976.56 2.444 92
in CDCl3
liquid film
4880 A,200 M,liquid
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