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109-01-3

1-Methylpiperazine

Product Name 1-Methylpiperazine

CAS109-01-3

MFC5H12N2

MW100.16

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  • 109-01-3_ms
    Mass

    MS-NW-1596          
    1-methylpiperazine
    C5H12N2             (Mass of molecular ion:    100)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       5.5
          18.0       1.9
          26.0       1.1
          27.0       3.9
          28.0      12.1
          29.0      10.3
          30.0       9.1
          41.0       3.7
          42.0      24.5
          43.0      35.2
          44.0      13.2
          45.0       1.4
          54.0       1.7
          55.0       1.5
          56.0      14.9
          57.0       9.6
          58.0     100.0
          59.0       3.5
          70.0       3.9
          71.0       2.2
         100.0      39.1
         101.0       2.4
    

90 MHz in CDCl3

  • 109-01-3_1hnmr

    1H NMR 89.56 MHz
    C5 H12 N2 0.04 ml : 0.5 ml CDCl3
    1-methylpiperazine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.884 B 2.369 C 2.264 D 1.72

         Hz     ppm     Int.
    

        264.13   2.950    109
        259.81   2.901    129
        254.63   2.844    213
        216.50   2.418    165
        213.38   2.383     74
        211.31   2.360    138
        206.75   2.309     97
        202.81   2.265   1000
        200.06   2.234     28
        154.13   1.721    123
    

in CDCl3

CCl4 solution

liquid film