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MS-NW-0848 N,N-diethyl-m-toluidine C11H17N (Mass of molecular ion: 163)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.8 28.0 6.0 29.0 3.3 32.0 1.2 39.0 3.2 41.0 1.6 42.0 1.1 51.0 2.0 63.0 1.8 65.0 6.9 77.0 3.7 78.0 1.4 79.0 1.3 81.5 1.0 89.0 1.9 90.0 1.2 91.0 17.0 92.0 3.1 93.0 2.8 104.0 1.2 105.0 1.8 117.0 1.1 118.0 7.8 119.0 4.7 120.0 27.3 121.0 2.5 132.0 2.2 133.0 1.9 134.0 3.4 148.0 100.0 149.0 11.2 162.0 4.2 163.0 34.1 164.0 4.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H17 N 0.04 ml : 0.5 ml CDCl3 N,N-diethyl-m-toluidine Assign. Shift(ppm)
A 7.174 B 6.60 C 6.57 D 3.406 E 2.383 F 1.228
Hz ppm Int.
650.81 7.267 64 647.25 7.228 22 644.63 7.198 58 642.31 7.172 78 639.50 7.141 35 634.94 7.090 81 590.81 6.597 282 583.81 6.519 107 316.06 3.530 127 309.00 3.451 426 302.00 3.373 458 295.00 3.294 159 213.50 2.384 755 117.06 1.308 505 110.06 1.229 1000 103.00 1.151 440
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