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90-90-4

4-BROMOBENZOPHENONE

Product Name 4-BROMOBENZOPHENONE

CAS90-90-4

MFC13H9BrO

MW261.11

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  • 90-90-4_ms
    Mass 

    MS-KW-0089          
4-bromobenzophenone
C13H9BrO            (Mass of molecular ion:    260)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          50.0       8.4
      51.0      12.1
      63.0       1.4
      74.0       3.3
      75.0      10.0
      76.0      15.7
      76.5       2.9
      77.0      36.1
      78.0       2.4
     104.0       2.1
     105.0     100.0
     106.0       7.8
     116.0       3.7
     117.0       3.5
     151.0       1.5
     152.0       3.7
     153.0       1.8
     155.0      12.6
     156.0       1.1
     157.0      12.3
     181.0      14.3
     182.0       2.2
     183.0      41.7
     184.0       3.5
     185.0      40.8
     186.0       3.2
     260.0      31.8
     261.0       5.0
     262.0      31.1
     263.0       4.5

400 MHz in CDCl3

90 MHz in CDCl3

  • 90-90-4_1hnmr_2

    1H NMR 399.65 MHz
    C13 H9 Br O 0.045 g : 0.5 ml CDCl3
    4-bromobenzophenone
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.772
      B             7.674
      C             7.63
      D             7.60
      E             7.488
  

         Hz     ppm     Int.


       3116.09   7.798     33
   3114.50   7.794     40
   3112.67   7.789     81
   3110.96   7.785    352
   3109.74   7.782    487
   3104.74   7.769    152
   3102.78   7.764    533
   3101.44   7.761    520
   3077.03   7.700     36
   3074.71   7.694     85
   3072.75   7.689    439
   3070.92   7.685    248
   3066.16   7.673    274
   3064.09   7.667   1000
   3057.74   7.652     38
   3057.37   7.651     38
   3052.37   7.638    206
   3050.54   7.634    990
   3048.46   7.628    366
   3045.90   7.622    117
   3043.70   7.616    244
   3041.87   7.612    472
   3039.31   7.605    145
   3037.11   7.600    294
   3035.40   7.596    151
   3031.01   7.585    125
   3029.66   7.581    219
   3028.56   7.579    153
   3001.10   7.510     94
   2999.39   7.506    374
   2998.17   7.502    245
   2991.82   7.487    561
   2985.96   7.472    102
   2984.25   7.468    224
   2983.76   7.466    199

  • 90-90-4_1hnmr

    1H NMR 89.56 MHz
    C13 H9 Br O 0.040 g : 0.5 ml CDCl3
    4-bromobenzophenone
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.78
      B             7.66
      C             7.63
      D          7.56 to 7.45
  

         Hz     ppm     Int.


        701.06   7.828    119
    699.44   7.810    143
    697.81   7.792     76
    696.88   7.782     70
    695.81   7.770     60
    694.00   7.749    189
    693.56   7.745    193
    691.44   7.721    246
    690.19   7.707     77
    689.13   7.695     47
    688.31   7.686     36
    687.25   7.674     49
    685.19   7.651   1000
    684.69   7.646    905
    684.25   7.641    943
    682.31   7.619    111
    681.31   7.608    131
    678.38   7.575     83
    677.63   7.567    176
    675.75   7.546    377
    673.38   7.519    153
    671.56   7.499     79
    669.75   7.479     83
    668.69   7.467    113
    668.06   7.460    137
    666.13   7.438     33
    662.44   7.397     45
    659.38   7.363     30

in CDCl3

  • 90-90-4_13cnmr

KBr disc

  • 90-90-4_ir1_2

Nujol

  • 90-90-4_ir2_1

  • 90-90-4_raman

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