-
MS-NW-0055 1-methylnaphthalene C11H10 (Mass of molecular ion: 142)
Source Temperature: 210 °C Sample Temperature: 55 °C Reservoir, 75 eV
18.0 1.4 28.0 1.0 39.0 2.6 50.0 1.5 51.0 2.4 57.5 5.3 58.0 1.0 62.0 1.5 63.0 4.3 65.0 1.6 69.0 1.4 69.5 3.1 70.0 3.7 70.5 3.9 71.0 6.4 74.0 1.7 75.0 1.6 77.0 1.7 87.0 1.1 89.0 3.4 91.0 4.1 106.0 1.8 113.0 1.3 115.0 21.7 116.0 2.4 126.0 1.0 139.0 8.6 140.0 2.1 141.0 78.4 142.0 100.0 143.0 11.3 147.0 4.8 148.0 4.2
400 MHz in CDCl3
-
1H NMR 399.65 MHz C11 H10 55.7 mg : 0.5 ml CDCl3 1-methylnaphthalene Assign. Shift(ppm)
A 7.958 B 7.808 C 7.672 D 7.48 E 7.45 F 7.336 G 7.279 J 2.654 THE SHIFT VALUES OF D,E WERE CALCULATED BY LAOCN PROGRAM.
Hz ppm Int.
3185.42 7.971 112 3184.20 7.968 124 3183.23 7.966 105 3178.47 7.954 63 3177.37 7.951 113 3176.39 7.948 136 3175.66 7.947 130 3125.85 7.822 120 3123.54 7.816 80 3118.16 7.803 167 3116.33 7.798 135 3070.56 7.684 124 3070.07 7.682 124 3062.50 7.663 138 3061.89 7.662 139 2997.92 7.502 66 2996.34 7.498 79 2991.09 7.485 163 2989.50 7.481 146 2988.16 7.477 66 2983.40 7.466 330 2981.32 7.460 317 2976.44 7.448 74 2975.46 7.446 140 2974.00 7.442 148 2968.63 7.429 69 2967.16 7.425 55 2940.06 7.357 124 2933.11 7.340 205 2924.93 7.319 194 2912.84 7.289 132 2911.74 7.286 173 2910.77 7.284 131 2905.88 7.272 76 2904.91 7.269 101 2903.81 7.266 71 1060.55 2.654 1000
More Suppliers