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N-Methylaniline

Product Name N-Methylaniline

CAS100-61-8

MFC7H9N

MW107.15

¹³CNMR

Mass

MS-NW-0684          
N-methylaniline
C7H9N               (Mass of molecular ion:    107)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      17.0       2.1
      18.0      10.3
      27.0       1.8
      30.0       3.3
      32.0       1.1
      37.0       1.3
      38.0       2.7
      39.0       7.5
      44.0       1.5
      50.0       5.0
      51.0      11.8
      52.0       4.8
      52.5       2.4
      53.0       5.3
      53.5       4.7
      54.0       1.2
      62.0       1.2
      63.0       3.1
      64.0       2.7
      65.0       8.3
      66.0       1.7
      74.0       1.9
      75.0       1.1
      76.0       1.2
      77.0      23.5
      78.0       8.3
      79.0      13.7
      80.0       1.3
      91.0       1.4
      92.0       2.1
     104.0       3.9
     105.0       2.0
     106.0     100.0
     107.0      80.0
     108.0       6.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₉ N	0.05 ml : 0.5 ml CDCl₃
N-methylaniline

    Assign.     Shift(ppm)

      A             7.164
      B             6.687
      C             6.558
      D             3.6
      E             2.743

     Hz     ppm     Int.

   2873.66   7.191     54
   2871.46   7.185    292
   2870.61   7.183    117
   2869.38   7.180    108
   2866.46   7.173     68
   2864.99   7.169    160
   2864.14   7.167    357
   2862.92   7.164    352
   2862.18   7.162    162
   2860.72   7.159     63
   2857.54   7.151    120
   2856.45   7.148    127
   2855.59   7.146    334
   2853.39   7.140     50
   2681.15   6.709     85
   2680.05   6.706    152
   2678.96   6.704     90
   2673.83   6.691    126
   2672.73   6.688    256
   2671.63   6.685    128
   2666.50   6.673     73
   2665.41   6.670    130
   2664.31   6.667     74
   2627.81   6.576     68
   2625.73   6.571    307
   2624.63   6.568    344
   2623.78   6.566    192
   2622.56   6.563    107
   2619.14   6.554    113
   2618.16   6.552    180
   2617.07   6.549    320
   2616.09   6.546    279
   2613.77   6.541     44
   1433.23   3.587     45
   1096.31   2.744   1000

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

OXIDATION WITH PBA IN ETHANOL

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