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1-(TRIISOPROPYLSILYL)PYRROLE

Product Name 1-(TRIISOPROPYLSILYL)PYRROLE

CAS87630-35-1

MFC13H25NSi

MW223.43

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  • Mass 

    MS-IW-9281          
1-(triisopropylsilyl)pyrrole
C13H25NSi           (Mass of molecular ion:    223)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          27.0       1.9
      39.0       2.0
      41.0       3.7
      42.0       1.3
      43.0       9.6
      44.0       2.3
      45.0       8.0
      53.0       1.7
      54.0       1.1
      55.0       3.5
      57.0       1.1
      58.0       1.5
      59.0      28.1
      60.0       2.3
      61.0       1.0
      62.0       3.2
      66.0       1.1
      67.0       9.9
      68.0       4.3
      69.0       7.6
      70.0       2.2
      71.0       8.9
      72.0       1.7
      73.0       6.3
      81.0       1.4
      82.0       1.8
      83.0      13.8
      84.0       3.0
      85.0      13.9
      86.0       1.8
      87.0       3.3
      94.0      17.6
      95.0       5.7
      96.0       8.5
      97.0       8.5
      98.0       1.9
      99.0       1.1
     109.0       1.9
     110.0      33.2
     111.0       7.8
     112.0       2.0
     113.0       4.5
     114.0       1.1
     122.0       1.5
     123.0       1.1
     124.0      26.5
     125.0       5.1
     126.0       1.3
     136.0       2.7
     137.0       1.1
     138.0      25.0
     139.0      22.1
     140.0       3.7
     152.0      43.9
     153.0       7.6
     154.0       2.1
     164.0       1.0
     180.0     100.0
     181.0      35.6
     182.0       7.6
     183.0       1.3
     222.0       1.6
     223.0      42.5
     224.0       8.6
     225.0       2.2

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H25 N Si 0.05 ml : 0.5 ml CDCl3
    1-(triisopropylsilyl)pyrrole
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.794
      B             6.312
      C             1.447
      D             1.097
  

         Hz     ppm     Int.


       2717.41   6.800    137
   2715.45   6.795    184
   2713.50   6.790    133
   2524.66   6.318    159
   2522.71   6.313    205
   2520.75   6.308    146
    594.60   1.488     46
    587.04   1.469    107
    579.47   1.450    149
    571.90   1.432    125
    564.45   1.413     75
    448.85   1.124     60
    442.26   1.107   1000
    434.57   1.088    921
    428.34   1.072     68

in CDCl3



liquid film





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