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87630-35-1

1-(TRIISOPROPYLSILYL)PYRROLE

Product Name 1-(TRIISOPROPYLSILYL)PYRROLE

CAS87630-35-1

MFC13H25NSi

MW223.43

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  • 87630-35-1_ms_1
    Mass

    MS-IW-9281          
    1-(triisopropylsilyl)pyrrole
    C13H25NSi           (Mass of molecular ion:    223)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.9
          39.0       2.0
          41.0       3.7
          42.0       1.3
          43.0       9.6
          44.0       2.3
          45.0       8.0
          53.0       1.7
          54.0       1.1
          55.0       3.5
          57.0       1.1
          58.0       1.5
          59.0      28.1
          60.0       2.3
          61.0       1.0
          62.0       3.2
          66.0       1.1
          67.0       9.9
          68.0       4.3
          69.0       7.6
          70.0       2.2
          71.0       8.9
          72.0       1.7
          73.0       6.3
          81.0       1.4
          82.0       1.8
          83.0      13.8
          84.0       3.0
          85.0      13.9
          86.0       1.8
          87.0       3.3
          94.0      17.6
          95.0       5.7
          96.0       8.5
          97.0       8.5
          98.0       1.9
          99.0       1.1
         109.0       1.9
         110.0      33.2
         111.0       7.8
         112.0       2.0
         113.0       4.5
         114.0       1.1
         122.0       1.5
         123.0       1.1
         124.0      26.5
         125.0       5.1
         126.0       1.3
         136.0       2.7
         137.0       1.1
         138.0      25.0
         139.0      22.1
         140.0       3.7
         152.0      43.9
         153.0       7.6
         154.0       2.1
         164.0       1.0
         180.0     100.0
         181.0      35.6
         182.0       7.6
         183.0       1.3
         222.0       1.6
         223.0      42.5
         224.0       8.6
         225.0       2.2
    

400 MHz in CDCl3

  • 87630-35-1_1hnmr_0

    1H NMR 399.65 MHz
    C13 H25 N Si 0.05 ml : 0.5 ml CDCl3
    1-(triisopropylsilyl)pyrrole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.794 B 6.312 C 1.447 D 1.097

         Hz     ppm     Int.
    

       2717.41   6.800    137
       2715.45   6.795    184
       2713.50   6.790    133
       2524.66   6.318    159
       2522.71   6.313    205
       2520.75   6.308    146
        594.60   1.488     46
        587.04   1.469    107
        579.47   1.450    149
        571.90   1.432    125
        564.45   1.413     75
        448.85   1.124     60
        442.26   1.107   1000
        434.57   1.088    921
        428.34   1.072     68
    

in CDCl3

  • 87630-35-1_13cnmr_0

liquid film

  • 87630-35-1_ir1_0

  • 87630-35-1_raman