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86608-70-0More Spectrum > 2-(1,3-Dioxolan-2-yl)ethyltriphenylphosphonium bromide(86608-70-0)MS
2-(1,3-Dioxolan-2-yl)ethyltriphenylphosphonium bromide
Product Name 2-(1,3-Dioxolan-2-yl)ethyltriphenylphosphonium bromide
CAS86608-70-0
MFC23H24BrO2P
MW443.31
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MS-IW-2174 (2-(1,3-dioxolan-2-yl)ethyl)triphenylphosphonium bromide C23H24BrO2P (Mass of molecular ion: 442)
Source Temperature: 200 °C Sample Temperature: 180 °C Direct, 75 eV
26.0 2.2 27.0 5.7 28.0 2.4 29.0 2.8 31.0 7.3 39.0 1.9 43.0 1.9 44.0 1.9 45.0 5.6 51.0 3.6 55.0 3.2 56.0 4.1 57.0 1.7 65.0 1.0 73.0 3.4 77.0 1.9 80.0 2.0 81.0 1.7 82.0 1.8 95.0 1.3 99.0 1.4 107.0 10.9 108.0 28.0 109.0 2.4 115.0 2.4 128.0 1.0 131.0 2.4 133.0 2.3 139.0 1.1 141.0 1.1 152.0 5.9 153.0 1.5 154.0 1.6 157.0 2.8 170.0 2.1 181.0 1.1 183.0 56.4 184.0 12.1 185.0 9.7 186.0 1.2 261.0 16.0 262.0 100.0 263.0 19.5 264.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C23 H24 Br O2 P 0.040 g : 0.5 ml CDCl3 (2-(1,3-dioxolan-2-yl)ethyl)triphenylphosphonium bromide Assign. Shift(ppm)
A 7.84 B 7.80 C 7.75 D 5.186 E *1 4.001 F *1 3.866 G 3.691 J 2.026
Hz ppm Int.
3145.02 7.870 74 3143.55 7.866 153 3141.36 7.861 168 3139.77 7.857 137 3138.67 7.854 132 3136.47 7.849 387 3135.38 7.846 267 3134.28 7.843 458 3131.96 7.837 239 3130.49 7.834 228 3129.03 7.830 567 3127.69 7.827 719 3125.85 7.822 308 3122.80 7.814 219 3120.73 7.809 824 3119.02 7.805 538 3116.82 7.799 202 3115.23 7.795 326 3113.65 7.791 187 3110.72 7.784 176 3108.40 7.778 901 3106.57 7.774 1000 3102.17 7.763 648 3099.73 7.757 495 3098.75 7.754 561 3094.97 7.745 569 3091.19 7.735 288 3090.09 7.732 223 3087.52 7.726 200 3086.43 7.723 145 3083.25 7.715 59 3082.15 7.713 50 2076.66 5.197 155 2072.88 5.187 344 2069.09 5.178 151 1607.54 4.023 136 1602.29 4.010 185 1600.34 4.005 344 1598.88 4.001 232 1596.80 3.996 182 1593.51 3.988 211 1582.89 3.961 48 1561.28 3.907 48 1550.66 3.881 219 1547.36 3.872 195 1545.29 3.867 244 1543.82 3.863 346 1541.87 3.859 171 1536.74 3.846 139 1490.36 3.730 96 1486.94 3.721 43 1484.74 3.716 59 1482.42 3.710 95 1479.49 3.702 74 1477.29 3.697 134 1474.24 3.689 137 1471.92 3.684 70 1469.24 3.677 95 1466.31 3.669 69 1461.18 3.657 101 824.22 2.063 62 820.56 2.054 75 819.09 2.050 52 815.06 2.040 118 811.40 2.031 120 809.69 2.026 96 807.86 2.022 117 806.03 2.017 86 804.20 2.013 116 800.29 2.003 53 798.71 1.999 76 795.04 1.990 62
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