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2-(1,3-Dioxolan-2-yl)ethyltriphenylphosphonium bromide

Product Name 2-(1,3-Dioxolan-2-yl)ethyltriphenylphosphonium bromide

CAS86608-70-0

MFC23H24BrO2P

MW443.31

¹³CNMR

Mass

MS-IW-2174          
(2-(1,3-dioxolan-2-yl)ethyl)triphenylphosphonium bromide
C23H24BrO2P         (Mass of molecular ion:    442)

   Source Temperature: 200 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      26.0       2.2
      27.0       5.7
      28.0       2.4
      29.0       2.8
      31.0       7.3
      39.0       1.9
      43.0       1.9
      44.0       1.9
      45.0       5.6
      51.0       3.6
      55.0       3.2
      56.0       4.1
      57.0       1.7
      65.0       1.0
      73.0       3.4
      77.0       1.9
      80.0       2.0
      81.0       1.7
      82.0       1.8
      95.0       1.3
      99.0       1.4
     107.0      10.9
     108.0      28.0
     109.0       2.4
     115.0       2.4
     128.0       1.0
     131.0       2.4
     133.0       2.3
     139.0       1.1
     141.0       1.1
     152.0       5.9
     153.0       1.5
     154.0       1.6
     157.0       2.8
     170.0       2.1
     181.0       1.1
     183.0      56.4
     184.0      12.1
     185.0       9.7
     186.0       1.2
     261.0      16.0
     262.0     100.0
     263.0      19.5
     264.0       1.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₃ H₂₄ Br O₂ P	0.040 g : 0.5 ml CDCl₃
(2-(1,3-dioxolan-2-yl)ethyl)triphenylphosphonium bromide

    Assign.     Shift(ppm)

      A             7.84
      B             7.80
      C             7.75
      D             5.186
      E     *1      4.001
      F     *1      3.866
      G             3.691
      J             2.026

     Hz     ppm     Int.

   3145.02   7.870     74
   3143.55   7.866    153
   3141.36   7.861    168
   3139.77   7.857    137
   3138.67   7.854    132
   3136.47   7.849    387
   3135.38   7.846    267
   3134.28   7.843    458
   3131.96   7.837    239
   3130.49   7.834    228
   3129.03   7.830    567
   3127.69   7.827    719
   3125.85   7.822    308
   3122.80   7.814    219
   3120.73   7.809    824
   3119.02   7.805    538
   3116.82   7.799    202
   3115.23   7.795    326
   3113.65   7.791    187
   3110.72   7.784    176
   3108.40   7.778    901
   3106.57   7.774   1000
   3102.17   7.763    648
   3099.73   7.757    495
   3098.75   7.754    561
   3094.97   7.745    569
   3091.19   7.735    288
   3090.09   7.732    223
   3087.52   7.726    200
   3086.43   7.723    145
   3083.25   7.715     59
   3082.15   7.713     50
   2076.66   5.197    155
   2072.88   5.187    344
   2069.09   5.178    151
   1607.54   4.023    136
   1602.29   4.010    185
   1600.34   4.005    344
   1598.88   4.001    232
   1596.80   3.996    182
   1593.51   3.988    211
   1582.89   3.961     48
   1561.28   3.907     48
   1550.66   3.881    219
   1547.36   3.872    195
   1545.29   3.867    244
   1543.82   3.863    346
   1541.87   3.859    171
   1536.74   3.846    139
   1490.36   3.730     96
   1486.94   3.721     43
   1484.74   3.716     59
   1482.42   3.710     95
   1479.49   3.702     74
   1477.29   3.697    134
   1474.24   3.689    137
   1471.92   3.684     70
   1469.24   3.677     95
   1466.31   3.669     69
   1461.18   3.657    101
    824.22   2.063     62
    820.56   2.054     75
    819.09   2.050     52
    815.06   2.040    118
    811.40   2.031    120
    809.69   2.026     96
    807.86   2.022    117
    806.03   2.017     86
    804.20   2.013    116
    800.29   2.003     53
    798.71   1.999     76
    795.04   1.990     62

in CDCl3

KBr disc

nujol mull

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