(+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL
Product Name (+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL
CAS86436-19-3
MFC30H20Cl2O2
MW483.38
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MassMS-IW-4043 (+)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol C30H20Cl2O2 (Mass of molecular ion: 482)
Source Temperature: 180 °C Sample Temperature: 170 °C Direct, 75 eV
18.0 5.1 39.0 1.0 49.0 1.7 50.0 8.1 51.0 11.3 63.0 1.9 74.0 2.3 75.0 10.2 76.0 7.3 77.0 46.2 78.0 4.1 87.0 1.6 88.0 3.3 93.5 1.0 94.0 1.6 99.0 1.3 100.0 3.1 100.5 1.6 101.0 9.0 101.5 2.0 105.0 100.0 105.5 1.0 106.0 8.7 106.5 2.2 107.0 1.3 111.0 16.9 112.0 1.9 113.0 5.6 125.0 1.7 126.0 4.3 127.0 2.1 137.0 1.4 139.0 51.2 140.0 4.1 141.0 16.6 142.0 1.3 150.0 1.3 151.0 2.4 152.0 4.3 153.0 1.9 154.0 4.4 155.0 3.1 160.0 1.6 163.0 1.1 176.0 1.0 180.0 1.1 181.0 4.8 187.0 1.2 188.0 5.5 189.0 2.8 190.0 2.0 199.0 1.0 200.0 3.9 201.0 5.6 202.0 32.2 203.0 21.0 204.0 3.3 211.0 1.8 212.0 1.5 213.0 5.5 214.0 1.6 215.0 1.4 216.0 42.9 217.0 6.4 218.0 14.2 219.0 2.1 230.0 3.7 231.0 40.1 232.0 7.4 238.0 1.4 249.0 1.9 265.0 4.6 266.0 1.3 267.0 1.6 343.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H20 Cl2 O2 0.039 g : 0.5 ml CDCl3 (+)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol 
Assign. Shift(ppm)
A 7.885 B 7.472 C 7.48 to 7.46 D 7.29 E 3.26
Hz ppm Int.3156.37 7.898 181 3155.27 7.896 142 3154.91 7.895 155 3151.49 7.886 55 3150.15 7.883 56 3148.93 7.880 171 3148.56 7.879 189 3146.61 7.874 173 2993.65 7.491 50 2991.94 7.487 274 2989.75 7.481 189 2987.79 7.477 121 2986.69 7.474 126 2985.84 7.472 169 2983.89 7.467 387 2982.30 7.463 360 2980.22 7.458 41 2979.13 7.455 45 2937.99 7.352 68 2936.28 7.348 51 2934.08 7.342 185 2932.25 7.338 187 2931.15 7.335 173 2929.69 7.331 397 2927.25 7.325 262 2926.27 7.323 201 2925.42 7.320 465 2924.44 7.318 362 2923.34 7.315 625 2922.97 7.314 621 2921.75 7.311 664 2918.70 7.304 351 2916.87 7.299 150 2912.60 7.288 243 2910.77 7.284 266 2908.33 7.278 72 2905.88 7.272 126 2904.42 7.268 105 2903.44 7.265 174 2897.71 7.251 74 2896.00 7.247 65 1301.51 3.257 1000
in CDCl3
KBr disc
nujol mull
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