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MS-IW-9307 1,1-diphenyl-2-propyn-1-ol C15H12O (Mass of molecular ion: 208)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.6 26.0 3.6 27.0 2.1 28.0 1.4 39.0 4.6 50.0 5.9 51.0 20.5 52.0 3.5 53.0 100.0 54.0 3.3 62.0 2.2 63.0 5.5 64.0 1.1 65.0 1.0 69.5 1.4 74.0 3.1 75.0 4.0 76.0 7.4 77.0 44.4 78.0 34.8 79.0 2.4 81.5 2.3 82.0 1.6 82.5 3.7 86.0 1.4 87.0 2.0 88.0 2.7 89.0 5.0 91.0 1.7 93.5 1.8 94.0 2.2 94.5 5.3 95.0 1.6 101.0 1.3 102.0 14.8 103.0 15.4 104.0 3.3 105.0 37.9 106.0 3.0 113.0 2.0 114.0 2.4 115.0 2.4 126.0 1.1 129.0 2.8 130.0 41.0 131.0 64.8 132.0 6.4 139.0 1.9 150.0 1.2 151.0 2.3 152.0 5.2 153.0 2.6 154.0 1.6 155.0 6.4 163.0 2.9 164.0 1.7 165.0 14.9 166.0 2.3 176.0 2.7 177.0 2.6 178.0 18.9 179.0 26.2 180.0 7.6 181.0 3.2 182.0 8.9 183.0 1.4 187.0 3.1 188.0 2.7 189.0 18.0 190.0 7.1 191.0 12.1 192.0 3.9 193.0 1.9 207.0 38.2 208.0 71.3 209.0 11.2 210.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H12 O 0.038 g : 0.5 ml CDCl3 1,1-diphenyl-2-propyn-1-ol Assign. Shift(ppm)
A 7.590 B 7.315 C 7.259 D 2.87 E 2.847
Hz ppm Int.
3039.92 7.607 517 3038.45 7.603 762 3036.38 7.598 194 3033.08 7.590 368 3031.49 7.586 725 3030.15 7.583 583 3027.83 7.577 99 2932.50 7.338 217 2931.27 7.335 341 2929.32 7.330 152 2926.51 7.323 163 2924.19 7.317 772 2922.61 7.313 381 2917.97 7.302 289 2916.50 7.298 545 2914.06 7.292 99 2911.50 7.286 37 2907.84 7.276 234 2906.37 7.273 403 2905.03 7.269 232 2901.61 7.261 146 2899.41 7.255 398 2896.48 7.248 93 2893.31 7.240 88 2891.97 7.237 133 2890.63 7.233 66 1147.71 2.872 685 1137.82 2.848 1000
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