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1-NAPHTHALENEACETAMIDE

Product Name 1-NAPHTHALENEACETAMIDE

CAS86-86-2

MFC12H11NO

MW185.22

¹HNMR

¹³CNMR

IR1

IR2

Mass

MS-NW-7979          
1-naphthaleneacetamide
C12H11NO            (Mass of molecular ion:    185)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.4
      39.0       3.5
      44.0       4.9
      50.0       1.6
      51.0       2.6
      57.5       4.6
      62.0       2.0
      63.0       5.5
      65.0       2.3
      69.0       1.2
      69.5       2.4
      70.0       1.2
      70.5       2.3
      74.0       1.6
      75.0       1.7
      76.0       1.0
      77.0       1.0
      86.0       1.0
      87.0       1.5
      88.0       1.0
      89.0       3.5
      91.0       1.4
     113.0       1.6
     114.0       1.2
     115.0      25.2
     116.0       2.7
     127.0       1.0
     139.0      11.1
     140.0       3.7
     141.0     100.0
     142.0      56.3
     143.0       6.3
     155.0       1.0
     185.0      44.5
     186.0       6.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₁₁ N O	0.035 g : 0.5 ml DMSO-d₆
1-naphthaleneacetamide

    Assign.     Shift(ppm)

      A             8.097
      B             7.916
      C             7.812
      D     *1      7.61
      E     *2      7.54
      F     *2      7.51
      G             7.454
      J             7.444
      K     *1      7.04
      L             3.886
     
     CONFIRMED BY LAOCN PROGRAM

     Hz     ppm     Int.

   3240.23   8.108    181
   3236.82   8.100     43
   3232.42   8.089    196
   3168.70   7.929    174
   3161.38   7.911    208
   3159.55   7.906    194
   3130.49   7.834     40
   3127.32   7.826    137
   3123.54   7.816    160
   3121.70   7.812    134
   3117.92   7.802    159
   3041.50   7.611    129
   3021.97   7.562     76
   3020.39   7.558     92
   3015.14   7.545    189
   3013.67   7.541    185
   3007.69   7.526    310
   3006.47   7.523    296
   3000.61   7.509    188
   2999.27   7.505    199
   2993.77   7.491     89
   2992.43   7.488     78
   2986.33   7.473     69
   2979.25   7.455    379
   2977.05   7.450    348
   2973.39   7.440    682
   2812.87   7.039    128
   1553.34   3.887   1000

in DMSO-d6

KBr disc

nujol mull

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