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MS-NW-1741 phenylacetamide C8H9NO (Mass of molecular ion: 135)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.0 27.0 1.7 28.0 5.0 32.0 1.1 37.0 1.1 38.0 3.3 39.0 16.6 40.0 1.5 41.0 3.4 44.0 21.1 50.0 4.6 51.0 8.1 52.0 2.3 61.0 1.5 62.0 4.2 63.0 10.7 64.0 3.1 65.0 25.2 66.0 1.8 74.0 1.0 77.0 2.2 89.0 7.6 90.0 5.0 91.0 100.0 92.0 91.6 93.0 6.7 117.0 1.5 135.0 17.6 136.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O 0.043 g : 0.5 ml CDCl3 phenylacetamide Assign. Shift(ppm)
A 7.52 to 7.07 B *1 5.9 C *1 5.5 D 3.57
Hz ppm Int.
665.94 7.436 38 663.44 7.408 54 661.63 7.388 63 657.19 7.338 236 654.63 7.310 1000 650.13 7.260 295 645.94 7.213 78 642.50 7.174 32 642.38 7.173 32 640.69 7.154 27 525.19 5.865 22 319.25 3.565 737
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