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MS-IW-1239 2-carbazolol C12H9NO (Mass of molecular ion: 183)
Source Temperature: 170 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 2.6 51.0 1.7 63.0 3.3 63.5 1.2 64.0 2.0 75.0 1.4 76.0 1.3 76.5 3.2 77.0 7.4 77.5 1.8 91.5 11.4 92.0 1.6 101.0 1.6 102.0 1.0 126.0 2.8 127.0 7.6 128.0 4.7 129.0 2.4 152.0 1.0 153.0 2.2 154.0 26.6 155.0 9.7 156.0 1.3 167.0 1.7 182.0 8.9 183.0 100.0 184.0 13.5 185.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H9 N O 0.037 g : 0.5 ml DMSO-d6 2-carbazolol Assign. Shift(ppm)
A 10.9 B 9.42 C 7.921 D 7.855 E 7.386 F 7.252 G 7.079 J 6.863 K 6.669
Hz ppm Int.
4375.46 10.949 375 3767.70 9.428 1000 3169.25 7.931 304 3161.47 7.911 317 3143.77 7.867 395 3135.38 7.846 414 2956.70 7.399 296 2948.61 7.378 394 2906.34 7.273 153 2905.43 7.270 192 2898.41 7.253 316 2891.54 7.236 147 2891.08 7.235 146 2890.32 7.233 178 2836.46 7.098 213 2829.28 7.080 326 2828.83 7.079 334 2821.50 7.060 172 2744.29 6.867 494 2742.16 6.862 598 2670.59 6.683 288 2668.46 6.677 323 2662.20 6.662 285 2660.06 6.656 323
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