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MassMS-NW-0378 carbazole C12H9N (Mass of molecular ion: 167)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
39.0 1.3 63.0 1.9 69.0 1.2 69.5 3.7 70.0 1.4 70.5 3.2 75.0 1.1 82.5 2.6 83.0 1.2 83.5 11.8 84.0 1.6 87.0 1.0 89.0 1.2 113.0 1.6 114.0 1.1 115.0 1.3 138.0 1.2 139.0 8.7 140.0 6.7 141.0 1.0 164.0 2.1 165.0 1.4 166.0 16.1 167.0 100.0 168.0 13.5 178.0 1.0
parameter in DMSO-d6
400 MHz in CDCl3
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1H NMR 300 MHz C12 H9 N 5 wt% in DMSO carbazole 
Parameter ppm Hz
D(A) 8.104 D(B) 7.158 D(C) 7.388 D(D) 7.502 D(E) 11.21 J(A,A') 0.0 J(A,B) 7.89 J(A,B') 0.0 J(A,C) 1.23 J(A,C') 0.0 J(A,D) 0.67 J(A,D') 0.0 J(A,E) 0.7 J(A',B) 0.0 J(A',B') 7.89 J(A',C) 0.0 J(A',C') 1.23 J(A',D) 0.0 J(A',D') 0.67 J(A',E) 0.7 J(B,B') 0.0 J(B,C) 7.24 J(B,C') 0.0 J(B,D) 0.96 J(B,D') 0.0 J(B,E) 0.0 J(B',C) 0.0 J(B',C') 7.24 J(B',D) 0.0 J(B',D') 0.96 J(B',E) 0.0 J(C,C') 0.0 J(C,D) 8.13 J(C,D') 0.0 J(C,E) 0.0 J(C',D) 0.0 J(C',D') 8.13 J(C',E) 0.0 J(D,D') 0.0 J(D,E) 0.0 J(D',E) 0.0 BALKAU,F. & HEFFERNAN,M.L. AUST.J.CHEM. 26, 1501 (1973)
Hz ppm Int.3363.05 11.210 955 2435.21 8.117 667 2427.34 8.091 709 2255.14 7.517 613 2247.07 7.490 1000 2224.38 7.415 476 2223.16 7.411 481 2217.16 7.391 623 2216.09 7.387 782 2209.09 7.364 369 2207.87 7.360 362 2155.14 7.184 495 2154.23 7.181 493 2147.16 7.157 813 2140.17 7.134 384 2139.17 7.131 377
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1H NMR 399.65 MHz C12 H9 N saturated in CDCl3 carbazole Assign. Shift(ppm)
A 8.084 B 8.03 C 7.42 D 7.42 E 7.24 CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.3236.08 8.098 116 3235.11 8.095 265 3234.38 8.094 282 3233.40 8.091 136 3228.27 8.078 128 3227.54 8.076 259 3226.44 8.074 254 3225.71 8.072 146 3207.89 8.027 30 2973.27 7.440 44 2972.41 7.438 47 2968.51 7.428 957 2967.53 7.426 1000 2965.09 7.420 499 2964.23 7.418 515 2963.62 7.416 531 2962.52 7.413 484 2955.57 7.396 55 2954.47 7.393 57 2906.13 7.272 42 2901.25 7.260 261 2897.95 7.252 258 2896.48 7.248 203 2893.43 7.240 305 2890.26 7.232 239 2888.55 7.228 194 2885.38 7.220 205
in CDCl3
KBr disc
nujol mull
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