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85417-41-0

TRIS(2,6-DIMETHOXYPHENYL)PHOSPHINE

Product Name TRIS(2,6-DIMETHOXYPHENYL)PHOSPHINE

CAS85417-41-0

MFC24H27O6P

MW442.44

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  • 85417-41-0_ms_1
    Mass 

    MS-IW-9301          
tris(2,6-dimethoxyphenyl)phosphine
C24H27O6P           (Mass of molecular ion:    442)


       Source Temperature: 130 °C
   Sample Temperature: 100 °C
   Direct, 75 eV


          18.0       1.3
      28.0       1.6
      39.0       1.3
      47.0       1.2
      65.0       1.6
      76.0       1.1
      77.0       3.9
      78.0       1.5
      79.0       1.3
      91.0      16.3
      92.0       2.3
      93.0       3.9
      94.0       1.1
      95.0       2.6
     105.0       1.1
     106.0       1.3
     107.0       4.3
     108.0       1.2
     109.0       2.5
     110.0       1.0
     115.0       1.0
     121.0      11.1
     122.0       1.5
     123.0       3.7
     124.0       1.3
     125.0       7.7
     126.0       1.0
     133.0       1.1
     135.0       1.5
     137.0       8.5
     138.0       3.2
     139.0       6.0
     149.0       1.1
     150.0       1.3
     151.0     100.0
     152.0      12.6
     153.0       8.1
     154.0       1.3
     155.0       3.0
     157.0       1.2
     165.0       2.0
     166.0       3.4
     167.0      17.1
     168.0       3.3
     169.0       4.6
     170.0       1.6
     171.0       1.2
     181.0       1.9
     182.0       1.3
     183.0       2.6
     195.0       1.1
     197.0       1.4
     199.0       1.6
     211.0       1.3
     213.0       3.1
     214.0       1.1
     215.0       1.6
     221.0       3.2
     225.0       1.0
     226.0       1.5
     227.0       1.4
     228.0       1.2
     229.0       2.1
     230.0       1.0
     231.0       1.0
     241.0       1.7
     242.0       1.1
     243.0       6.9
     244.0       1.9
     245.0       2.3
     255.0       3.1
     256.0       1.1
     257.0       3.3
     258.0       1.4
     259.0       3.0
     261.0       1.0
     273.0       5.0
     274.0       1.2
     275.0       1.3
     289.0       3.1
     290.0       1.3
     291.0      22.8
     292.0       3.7
     293.0       5.1
     303.0       1.0
     305.0       2.8
     306.0       2.4
     381.0       1.8
     393.0       2.5
     411.0       8.2
     412.0       2.1
     427.0       1.0
     442.0      13.8
     443.0       3.5

400 MHz in CDCl3

  • 85417-41-0_1hnmr_0

    1H NMR 399.65 MHz
    C24 H27 O6 P 0.041 g : 0.5 ml CDCl3
    tris(2,6-dimethoxyphenyl)phosphine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.122
      B             6.435
      C             3.470
  

         Hz     ppm     Int.


       2855.22   7.145     39
   2854.25   7.142     37
   2846.92   7.124     78
   2846.07   7.122     75
   2838.75   7.104     44
   2837.77   7.101     42
   2577.39   6.450    141
   2574.46   6.442    138
   2569.21   6.429    133
   2566.28   6.422    132
   1386.84   3.471   1000

in CDCl3

  • 85417-41-0_13cnmr_0

  • 85417-41-0_pnmr

KBr disc

  • 85417-41-0_ir1_2

nujol mull

  • 85417-41-0_ir2_1

  • 85417-41-0_raman

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