2-CYCLOHEXEN-1-OL

Mass

MS-KW-0253          
2-cyclohexen-1-ol
C6H10O              (Mass of molecular ion:     98)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.8
      17.0       2.6
      18.0       9.8
      26.0       3.3
      27.0      20.0
      28.0       4.6
      29.0      11.2
      31.0       4.2
      37.0       2.4
      38.0       5.0
      39.0      32.3
      40.0       7.0
      41.0      28.7
      42.0      16.9
      43.0      16.1
      44.0       4.5
      47.0       1.0
      49.0       1.3
      50.0       9.0
      51.0      14.2
      52.0      10.0
      53.0      10.2
      54.0      10.8
      55.0      30.2
      56.0       5.3
      57.0      13.6
      58.0       1.1
      62.0       1.1
      63.0       2.2
      65.0       5.7
      66.0       1.9
      67.0       9.0
      68.0       3.6
      69.0      22.9
      70.0     100.0
      71.0       5.2
      74.0       2.2
      75.0       1.2
      77.0      33.9
      78.0      13.8
      79.0      78.4
      80.0      38.9
      81.0       6.6
      82.0       2.3
      83.0      35.3
      84.0       2.0
      95.0       1.2
      97.0      29.7
      98.0      35.5
      99.0       2.8

Assign. Shift(ppm) A 5.800 B 5.739 C 4.179 D 2.8 E *1 2.02 F *1 1.86 G *2 1.74 J *2 1.61 K *2 1.57 assigned by C-H COSY

     Hz     ppm     Int.

   2329.23   5.827    181
   2328.13   5.824    182
   2325.81   5.818    306
   2324.59   5.815    288
   2322.27   5.809    184
   2321.17   5.807    175
   2319.22   5.802    314
   2318.00   5.799    326
   2315.68   5.793    570
   2314.46   5.790    569
   2312.14   5.784    336
   2311.04   5.781    329
   2300.66   5.755    311
   2298.71   5.750    516
   2295.90   5.743    483
   2293.71   5.738    250
   2288.70   5.725    249
   2285.77   5.718    260
   2283.57   5.713    145
   1672.49   4.184    395
   1671.51   4.182    383
   1669.44   4.176    344
   1668.46   4.174    304
   1109.50   2.776   1000
    824.83   2.064     86
    822.88   2.059    104
    821.54   2.055    107
    819.46   2.050    121
    817.51   2.045    114
    815.56   2.040    106
    812.38   2.033    129
    810.31   2.027    173
    808.23   2.022    163
    806.89   2.019    237
    804.94   2.014    249
    803.23   2.010    316
    801.40   2.005    306
    799.44   2.000    316
    797.49   1.995    279
    795.54   1.990    177
    793.95   1.986    216
    792.00   1.982    208
    790.41   1.978    180
    788.58   1.973    241
    786.38   1.968    293
    783.70   1.961    323
    782.84   1.959    294
    780.40   1.953    270
    778.69   1.948    193
    776.98   1.944    159
    770.39   1.928    105
    768.32   1.922    124
    764.78   1.913    130
    761.11   1.904    192
    758.67   1.898    193
    755.74   1.891    159
    753.55   1.885    185
    749.64   1.876    283
    744.76   1.863    291
    740.12   1.852    297
    735.11   1.839    216
    727.18   1.819     73
    716.92   1.794     62
    709.48   1.775    121
    703.62   1.760    261
    701.05   1.754    192
    699.10   1.749    235
    693.00   1.734    296
    687.50   1.720    209
    685.06   1.714    202
    682.74   1.708    192
    678.84   1.699     97
    676.40   1.692    104
    656.74   1.643    194
    654.18   1.637     98
    650.40   1.627    202
    647.59   1.620    320
    645.15   1.614    311
    641.12   1.604    355
    639.04   1.599    410
    638.07   1.597    415
    634.89   1.589    468
    633.43   1.585    429
    632.09   1.582    433
    630.99   1.579    361
    629.16   1.574    432
    626.96   1.569    363
    623.42   1.560    226
    621.22   1.554    194
    620.00   1.551    206
    617.56   1.545    179
    614.26   1.537    169
    612.07   1.531     99
    610.72   1.528     90
    607.67   1.520     71
    605.11   1.514     75