(S)-(-)-1-METHYL-2-(1-NAPHTHYLAMINOMETHYL)PYRROLIDINE
Product Name (S)-(-)-1-METHYL-2-(1-NAPHTHYLAMINOMETHYL)PYRROLIDINE
CAS82160-07-4
MFC16H20N2
MW240.34
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MassMS-IW-4912 (S)-N-(1-methyl-2-pyrrolidinylmethyl)-1-naphthylamine C16H20N2 (Mass of molecular ion: 240)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 2.1 42.0 5.5 82.0 3.0 83.0 1.2 84.0 100.0 85.0 6.3 115.0 1.6 127.0 2.2 128.0 1.4 143.0 1.1 154.0 1.6 155.0 1.0 240.0 6.8 241.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H20 N2 0.039 g : 0.5 ml CDCl3 (S)-N-(1-methyl-2-pyrrolidinylmethyl)-1-naphthylamine 
Assign. Shift(ppm)
A 7.838 B 7.768 C 7.43 D 7.41 E 7.335 F 7.198 G 6.564 J 5.08 K *1 3.30 L *1 3.240 M *2 3.159 N 2.571 P 2.336 Q *2 2.274 R *3 1.95 S *4 1.90 T *3 1.83 U *4 1.75
Hz ppm Int.3137.70 7.852 67 3137.08 7.850 63 3134.03 7.842 38 3133.18 7.840 40 3131.10 7.835 59 3130.13 7.833 53 3128.17 7.828 72 3109.25 7.780 73 3106.93 7.775 59 3105.96 7.772 58 3104.13 7.768 48 3101.20 7.760 63 3099.85 7.757 85 2976.07 7.447 33 2971.19 7.435 111 2969.24 7.430 175 2965.45 7.421 195 2961.55 7.411 158 2959.47 7.406 96 2954.71 7.394 32 2940.06 7.357 75 2932.13 7.337 140 2924.44 7.318 105 2880.25 7.207 133 2872.19 7.187 96 2627.08 6.574 111 2619.63 6.555 107 2029.54 5.079 32 1315.67 3.293 44 1314.09 3.289 42 1312.26 3.284 47 1300.90 3.256 67 1296.39 3.244 70 1284.67 3.215 30 1271.12 3.181 37 1269.78 3.178 35 1269.53 3.177 35 1262.33 3.159 68 1255.00 3.141 48 1032.10 2.583 43 1028.44 2.574 44 1026.98 2.570 40 1024.41 2.564 47 933.84 2.337 1000 922.24 2.308 50 914.67 2.289 53 912.60 2.284 76 905.27 2.266 73 903.44 2.261 59 896.00 2.242 34 787.11 1.970 42 785.40 1.966 44 778.93 1.950 50 776.86 1.944 47 771.85 1.932 36 768.68 1.924 30 766.11 1.917 48 764.16 1.913 42 762.21 1.908 45 759.28 1.900 39 754.64 1.889 55 750.85 1.879 40 749.27 1.875 34 747.07 1.870 58 742.19 1.858 35 740.36 1.853 46 737.67 1.846 34 730.59 1.829 54 704.35 1.763 40 702.64 1.759 47 700.68 1.754 45 693.12 1.735 37 691.28 1.730 30
in CDCl3
KBr disc
nujol mull
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