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1-Methylpyrrolidine

Product Name 1-Methylpyrrolidine

CAS120-94-5

MFC5H11N

MW85.15

¹³CNMR

Mass

MS-NW-3530          
N-methylpyrrolidine
C5H11N              (Mass of molecular ion:     85)

   Source Temperature: 290 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0      12.8
      18.0       3.3
      26.0       2.1
      27.0       8.6
      28.0       8.0
      29.0       3.6
      30.0       4.2
      38.0       1.0
      39.0       6.7
      40.0       1.9
      41.0      10.7
      42.0     100.0
      43.0       9.4
      44.0       3.7
      53.0       1.1
      54.0       2.4
      55.0       6.6
      56.0       3.3
      57.0      89.7
      58.0       4.2
      67.0       1.9
      68.0       1.5
      69.0       1.0
      70.0       1.5
      82.0       9.4
      83.0       2.0
      84.0      97.2
      85.0      55.8
      86.0       3.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₁ N	0.04 ml : 0.5 ml CDCl₃
N-methylpyrrolidine

    Assign.     Shift(ppm)

      A             2.47
      B             2.353
      C             1.78

     Hz     ppm     Int.

    228.06   2.547     35
    224.81   2.511     67
    223.56   2.497     67
    220.88   2.467    142
    218.88   2.444    105
    217.19   2.426     65
    217.00   2.423     65
    215.50   2.407     69
    214.31   2.393     77
    210.81   2.354   1000
    208.38   2.327     38
    166.19   1.856     88
    163.19   1.823     98
    162.13   1.811     79
    159.50   1.781    233
    157.63   1.761     68
    155.88   1.741    113
    154.50   1.726     43
    152.81   1.707     63

in CDCl3

liquid film

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