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82-02-0

KHELLIN

Product Name KHELLIN

CAS82-02-0

MFC14H12O5

MW260.24

More

  • 82-02-0_ms
    Mass

    MS-IW-9456          
    4,9-dimethoxy-7-methylfuro(3,2-g)chromen-5-one
    C14H12O5            (Mass of molecular ion:    260)
    

       Source Temperature: 170 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          15.0       4.2
          18.0       2.6
          27.0       2.5
          28.0       5.9
          29.0       2.0
          37.0       1.3
          38.0       5.0
          39.0       8.9
          40.0       2.0
          43.0      12.1
          50.0       2.6
          51.0       5.8
          52.0       1.3
          53.0       4.5
          55.0       1.7
          59.0       1.0
          61.0       2.8
          62.0       5.0
          63.0       5.1
          64.0       1.4
          65.0       3.8
          66.0       9.2
          67.0       8.7
          68.0       2.2
          69.0       2.4
          73.0       1.7
          74.0       2.9
          75.0       3.8
          76.0       2.1
          77.0       8.3
          78.0       2.9
          79.0       2.3
          80.0       1.0
          81.0       4.2
          83.0       2.2
          86.0       1.4
          87.0       3.2
          88.0       1.1
          89.0       3.2
          90.0       4.5
          91.0       3.7
          92.0       3.6
          93.0       3.1
          94.0       6.3
          95.0       5.3
         101.0       3.3
         102.0       3.8
         103.0       1.7
         104.0       1.2
         105.0      14.0
         106.0       3.4
         107.0       1.1
         109.0       1.7
         115.0       2.0
         116.0       1.3
         117.0       1.6
         118.0       3.6
         119.0       5.2
         120.0       1.2
         121.0       2.7
         122.0       1.8
         123.0       1.6
         130.0       7.5
         130.5       1.1
         131.0       1.9
         132.0       1.4
         133.0       2.8
         134.0       4.9
         143.0       1.1
         145.0       1.5
         146.0       1.6
         147.0      11.8
         148.0       1.6
         149.0       3.3
         150.0       3.1
         151.0       1.5
         153.0       2.4
         159.0       1.7
         160.0       2.7
         161.0       4.8
         162.0       4.1
         163.0       1.7
         171.0       1.4
         173.0       3.3
         174.0       2.8
         175.0      13.4
         176.0       2.0
         177.0      19.1
         178.0       2.1
         184.0       1.4
         186.0       1.0
         187.0       2.0
         188.0       1.0
         189.0      29.2
         190.0       5.0
         191.0       1.8
         199.0       1.1
         201.0       4.6
         202.0       6.0
         203.0       1.6
         205.0       5.0
         214.0       3.5
         215.0       6.8
         216.0      78.8
         217.0      47.4
         218.0       6.3
         219.0       1.0
         227.0       7.9
         228.0       2.4
         229.0       2.0
         230.0       4.9
         231.0      39.6
         232.0       5.9
         243.0       2.4
         244.0       2.9
         245.0     100.0
         246.0      14.6
         247.0       2.1
         259.0       4.8
         260.0      89.9
         261.0      15.7
         262.0       2.2
    

400 MHz in CDCl3

  • 82-02-0_1hnmr

    1H NMR 399.65 MHz
    C14 H12 O5 0.040 g : 0.5 ml CDCl3
    4,9-dimethoxy-7-methylfuro(3,2-g)chromen-5-one
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.639 B 7.023 C 6.062 D 4.199 E 4.064 F 2.400

         Hz     ppm     Int.
    

       3054.32   7.643    206
       3052.12   7.637    208
       2808.11   7.027    208
       2805.91   7.021    201
       2423.22   6.064    165
       2422.49   6.062    169
       1678.10   4.199   1000
       1624.15   4.064    969
        959.59   2.402    534
        958.86   2.400    533
    

in CDCl3

  • 82-02-0_13cnmr

KBr disk

  • 82-02-0_ir1_2

nujol mull

  • 82-02-0_ir2