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N-Methylacetamide

Product Name N-Methylacetamide

CAS79-16-3

MFC3H7NO

MW73.09

¹³CNMR

Mass

MS-NW-4322          
N-methylacetamide
C3H7NO              (Mass of molecular ion:     73)

   Source Temperature: 230 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      13.0       1.1
      14.0       4.6
      15.0      32.2
      17.0       1.1
      18.0       5.3
      26.0       1.0
      27.0       2.4
      28.0      21.3
      29.0       2.6
      30.0      87.3
      31.0      22.2
      32.0       5.8
      40.0       1.0
      41.0       1.7
      42.0      10.6
      43.0     100.0
      44.0       3.3
      45.0       6.4
      54.0       1.1
      58.0      45.2
      59.0       1.2
      73.0      93.3
      74.0       3.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₃ H₇ N O	0.02 ml : 0.5 ml CDCl₃
N-methylacetamide

    Assign.     Shift(ppm)

      A             6.4
      B             2.786
      C             1.983

     Hz     ppm     Int.

    252.06   2.815    538
    251.69   2.811    496
    247.25   2.761    529
    246.88   2.757    481
    177.69   1.985   1000

in CDCl3

liquid film

4880 A,200 M,liquid

OXIDATION OF N-METHYLACETAMIDE WITH TICL3-H2O2 SYSTEM

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