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MS-NW-8533 dimethyldiphenylsilane C14H16Si (Mass of molecular ion: 212)
Source Temperature: 250 °C Sample Temperature: 140 °C Reservoir, 75 eV
43.0 5.0 51.0 1.0 53.0 4.4 67.0 1.3 77.0 1.0 79.0 2.2 91.0 2.4 93.0 3.5 98.0 1.2 103.0 1.1 105.0 9.7 106.0 2.0 107.0 2.2 119.0 4.2 120.0 1.0 135.0 6.1 155.0 1.0 165.0 3.4 180.0 1.5 181.0 3.5 193.0 1.2 195.0 4.9 196.0 1.2 197.0 100.0 198.0 19.4 199.0 4.9 212.0 13.4 213.0 2.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H16 Si 0.05 ml : 0.5 ml CDCl3 dimethyldiphenylsilane Assign. Shift(ppm)
A 7.52 B 7.33 C 7.28 D 0.535 CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.
677.75 7.568 59 675.94 7.548 60 674.94 7.537 82 673.81 7.524 56 672.44 7.509 82 671.44 7.498 104 669.81 7.479 86 668.31 7.463 129 666.56 7.443 61 664.69 7.422 40 660.69 7.378 51 659.88 7.369 56 659.25 7.361 64 658.31 7.351 86 657.06 7.337 251 655.50 7.320 115 654.31 7.306 187 652.69 7.288 104 650.63 7.265 149 648.06 7.237 36 51.25 0.573 70 47.94 0.536 1000 44.63 0.499 44
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