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MassMS-NW-8529 methyldiphenylsilane C13H14Si (Mass of molecular ion: 198)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
39.0 1.0 43.0 6.8 51.0 2.2 53.0 9.6 54.0 1.1 55.0 1.4 66.0 1.1 67.0 1.9 69.0 1.2 77.0 2.4 78.0 1.4 79.0 6.0 91.0 2.3 93.0 3.2 95.0 1.4 98.0 2.1 103.0 2.9 105.0 51.4 106.0 6.4 107.0 2.3 119.0 2.9 120.0 100.0 121.0 17.9 122.0 4.6 129.0 1.5 152.0 1.3 153.0 1.4 154.0 2.3 155.0 2.7 165.0 2.2 179.0 1.0 180.0 3.0 181.0 10.2 182.0 2.4 183.0 33.3 184.0 6.1 185.0 1.6 195.0 2.3 197.0 10.6 198.0 25.2 199.0 5.1 200.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C13 H14 Si 0.05 ml : 0.5 ml CDCl3 methyldiphenylsilane 
Assign. Shift(ppm)
A 7.54 B 7.34 C 7.32 D 4.951 E 0.601 CONFIRMED BY LAOCN CALCULATION
Hz ppm Int.683.63 7.634 39 683.50 7.632 39 680.69 7.601 206 678.00 7.571 262 676.44 7.553 180 674.75 7.535 406 673.69 7.523 245 672.50 7.509 272 671.13 7.494 453 669.94 7.481 167 669.13 7.472 147 667.13 7.449 107 665.56 7.432 69 664.56 7.421 68 662.50 7.398 160 661.25 7.384 209 658.81 7.357 1000 656.25 7.328 745 654.25 7.306 385 652.25 7.283 435 650.25 7.261 101 649.13 7.248 108 644.75 7.200 32 644.00 7.191 31 449.25 5.017 59 445.44 4.974 171 441.63 4.932 173 437.75 4.888 61 59.19 0.661 49 55.75 0.623 937 51.88 0.580 905 48.38 0.541 46
in CDCl3
liquid film
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