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77317-55-6

Methyl 2-amino-5-iodobenzoate

Product Name Methyl 2-amino-5-iodobenzoate

CAS77317-55-6

MFC8H8INO2

MW277.06

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  • 77317-55-6_ms_1
    Mass

    MS-IW-9530          
    methyl 5-iodoanthranilate
    C8H8INO2            (Mass of molecular ion:    277)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.1
          28.0       2.4
          29.0       1.2
          37.0       1.6
          38.0       3.3
          39.0       3.6
          40.0       1.6
          41.0       4.4
          44.0       1.0
          45.5       1.4
          50.0       1.3
          51.0       1.6
          52.0      10.3
          53.0       1.6
          61.0       2.2
          62.0       5.7
          63.0      17.1
          64.0       8.6
          65.0       4.9
          74.0       1.3
          75.0       2.2
          77.0       1.1
          78.0       1.1
          79.0       1.6
          89.0       2.9
          90.0      18.6
          91.0      22.6
          92.0       3.4
         107.0       2.9
         108.5       2.4
         109.0       5.1
         117.0       1.1
         118.0       1.2
         119.0       1.4
         122.5       2.7
         123.0       4.3
         127.0       2.8
         128.0       2.5
         135.0       5.4
         138.5       4.1
         150.0       2.7
         191.0       1.3
         216.0       1.7
         217.0      17.6
         218.0      18.7
         219.0       1.8
         245.0      83.5
         246.0      20.6
         247.0       1.6
         277.0     100.0
         278.0       9.3
    

400 MHz in CDCl3

  • 77317-55-6_1hnmr_0

    1H NMR 399.65 MHz
    C8 H8 I N O2 0.037 g : 0.5 ml CDCl3
    methyl 5-iodoanthranilate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.132 B 7.466 C 6.451 D 5.77 E 3.860

         Hz     ppm     Int.
    

       3251.34   8.136    176
       3249.15   8.130    182
       2989.38   7.480    103
       2987.18   7.475    101
       2980.71   7.459    105
       2978.52   7.453    104
       2582.40   6.462    171
       2573.73   6.440    164
       2307.37   5.774     37
       1542.97   3.861   1000
    

in CDCl3

  • 77317-55-6_13cnmr_0

KBr disc

  • 77317-55-6_ir1_2

nujol mull

  • 77317-55-6_ir2_1