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77-99-6

Trimethylolpropane

Product Name Trimethylolpropane

CAS77-99-6

MFC6H14O3

MW134.17

More

  • 77-99-6_ms_1
    Mass

    MS-NW-0219          
    2-ethyl-2-hydroxymethyl-1,3-propanediol
    C6H14O3             (Mass of molecular ion:    134)
    

       Source Temperature: 180 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          15.0       2.1
          19.0       6.3
          26.0       1.0
          27.0      17.2
          28.0       3.4
          29.0      42.5
          30.0       1.1
          31.0      33.5
          39.0      15.5
          40.0       3.2
          41.0      43.0
          42.0       5.7
          43.0      23.7
          44.0      14.6
          45.0       6.4
          47.0       2.4
          51.0       1.0
          53.0       7.1
          54.0       2.1
          55.0      33.8
          56.0       5.0
          57.0     100.0
          58.0       8.7
          59.0       1.4
          61.0       2.3
          65.0       1.3
          67.0       9.4
          68.0      14.5
          69.0       8.5
          70.0      11.2
          71.0      22.2
          72.0       1.7
          73.0       2.3
          81.0       1.1
          83.0       5.5
          84.0       1.2
          85.0       7.4
          86.0      51.2
          87.0       3.3
          98.0       1.4
          99.0       1.2
         117.0       1.3
         135.0       2.7
    

90 MHz in D2O

  • 77-99-6_1hnmr_0

    1H NMR 89.56 MHz
    C6 H14 O3 0.044 g : 0.5 ml D2O
    2-ethyl-2-hydroxymethyl-1,3-propanediol
    ChemicalStructure
        Assign.     Shift(ppm)
    B 3.507 C 1.31 D 0.86 THE SOLVENT SIGNAL REMOVED.

         Hz     ppm     Int.
    

        314.19   3.509   1000
        122.75   1.371     56
        117.25   1.310     29
        114.88   1.283     87
        108.81   1.215     38
        107.38   1.199     37
         83.44   0.932    102
         76.63   0.856    176
         68.69   0.767     47
    

in D2O

KBr disc

liquid film

nujol mull

4880 A,200 M,powder