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1-Bromoadamantane

CAS768-90-1

MFC10H15Br

MW215.13

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  • Mass

    MS-KW-0260          
    1-bromotricyclo(3.3.1.1(3,7))decane
    C10H15Br            (Mass of molecular ion:    214)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       2.8
          29.0       1.4
          39.0       5.6
          41.0       6.0
          43.0       1.0
          51.0       1.9
          52.0       1.1
          53.0       3.1
          55.0       4.3
          65.0       3.5
          66.0       1.6
          67.0       7.7
          69.0       2.1
          77.0       6.6
          78.0       2.4
          79.0      20.3
          80.0       2.0
          81.0       6.0
          91.0       5.8
          92.0       2.0
          93.0      16.6
          94.0       2.0
          95.0       4.5
         105.0       1.2
         107.0       5.8
         135.0     100.0
         136.0      11.3
         152.0       1.0
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10H15Br 0.040 g : 0.5 ml CDCl3
    1-bromoadamantane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.367 B 2.104 C 1.73

         Hz     ppm     Int.
    

        947.51   2.371   1000
        944.22   2.362    971
        841.07   2.104    284
        694.95   1.739    683
        691.90   1.731    964
        688.48   1.723    563
    


  • 1H NMR 89.56 MHz
    C10 H15 Br 0.046 g : 0.5 ml CDCl3
    1-bromotricyclo(3.3.1.1(3,7))decane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.363 B 2.10 C 1.73 J(A,B)=3.0HZ. J(B,C)=3.0HZ.

         Hz     ppm     Int.
    

        213.38   2.383    768
        210.38   2.350   1000
        200.81   2.243     50
        188.25   2.102    263
        157.88   1.763    578
        155.00   1.731    871
        151.94   1.697    471
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder