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MS-NW-2938 1-ethylpiperidine C7H15N (Mass of molecular ion: 113)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.1 27.0 6.7 28.0 7.8 29.0 6.5 30.0 4.8 39.0 3.5 41.0 10.4 42.0 24.1 43.0 2.5 44.0 6.8 54.0 1.8 55.0 10.7 56.0 8.3 57.0 11.5 58.0 2.5 69.0 3.4 70.0 4.4 71.0 1.5 72.0 2.5 84.0 7.5 96.0 1.6 98.0 100.0 99.0 6.7 112.0 19.9 113.0 18.4 114.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H15 N 0.05 ml : 0.5 ml CDCl3 1-ethylpiperidine Assign. Shift(ppm)
A 2.37 B 2.35 C 1.72 to 1.34 D 1.076
Hz ppm Int.
222.81 2.488 114 222.19 2.481 111 215.13 2.403 585 212.63 2.375 339 207.88 2.322 716 201.19 2.247 176 200.63 2.241 156 153.81 1.718 60 148.13 1.654 141 143.50 1.603 208 142.31 1.589 229 135.69 1.516 306 134.75 1.505 314 128.56 1.436 85 127.00 1.419 68 124.69 1.393 50 124.38 1.389 51 102.88 1.149 486 95.88 1.071 1000 88.50 0.989 357
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