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7583-53-1More Spectrum > 1-Methyl-3-piperidinemethanol(7583-53-1)1HNMR
1-Methyl-3-piperidinemethanol
Product Name 1-Methyl-3-piperidinemethanol
CAS7583-53-1
MFC7H15NO
MW129.2
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MassMS-NW-5470 1-methyl-3-piperidinemethanol C7H15NO (Mass of molecular ion: 129)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 8.3 17.0 1.2 18.0 5.1 26.0 1.3 27.0 10.0 28.0 8.9 29.0 7.3 30.0 5.8 31.0 7.9 32.0 1.0 38.0 1.0 39.0 11.3 40.0 2.3 41.0 23.9 42.0 53.9 43.0 97.0 44.0 69.4 45.0 3.9 51.0 1.4 52.0 1.3 53.0 4.0 54.0 3.1 55.0 8.4 56.0 5.1 57.0 24.9 58.0 92.2 59.0 4.3 65.0 1.6 66.0 1.1 67.0 3.8 68.0 5.6 69.0 4.1 70.0 27.8 71.0 23.8 72.0 3.7 79.0 1.1 80.0 2.3 81.0 2.2 82.0 7.3 83.0 2.3 84.0 20.0 85.0 3.2 86.0 10.0 87.0 1.0 93.0 1.5 94.0 4.0 95.0 1.6 96.0 15.4 97.0 6.5 98.0 28.4 99.0 10.3 100.0 10.0 101.0 1.6 108.0 2.5 109.0 1.6 110.0 10.1 111.0 7.1 112.0 20.2 113.0 2.1 114.0 4.6 126.0 1.0 128.0 100.0 129.0 64.4 130.0 5.4 142.0 1.0
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C7 H15 N O 0.04 ml : 0.5 ml CDCl3 1-methyl-3-piperidinemethanol 
Assign. Shift(ppm)
A 3.86 B *1 3.51 C *1 3.45 D 2.89 E 2.69 F 2.246 G 2.04 to 1.54 J 0.97
Hz ppm Int.345.50 3.858 69 315.88 3.528 63 312.88 3.494 74 310.69 3.470 78 306.88 3.427 59 253.44 2.830 36 201.25 2.248 1000 167.31 1.869 37 163.63 1.828 65 163.50 1.826 65 162.81 1.818 65 157.19 1.756 102 155.94 1.742 89 152.13 1.699 73 149.38 1.668 73 146.00 1.631 79 141.81 1.584 33
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1H NMR 399.65 MHz C7 H15 N O 0.05 ml : 0.5 ml CDCl3 1-methyl-3-piperidinemethanol Assign. Shift(ppm)
A 4.9 B *1 3.480 C *1 3.373 D 2.916 E 2.745 F 2.247 G 1.92 J 1.78 K 1.75 to 1.66 L 1.59 M 0.934 ASSIGNED BY H-H COSY. J(B,C)=-10.6HZ. J(B,J)=5.4HZ. J(C,J)=6.9HZ.
Hz ppm Int.1399.78 3.503 66 1394.53 3.490 65 1389.16 3.476 108 1383.79 3.463 98 1355.96 3.393 89 1349.12 3.376 86 1345.34 3.367 66 1338.38 3.349 58 1170.17 2.928 50 1160.52 2.904 53 1102.54 2.759 44 1097.53 2.747 33 1091.43 2.731 45 898.32 2.248 1000 777.47 1.946 30 767.58 1.921 53 767.09 1.920 53 756.35 1.893 31 720.34 1.803 34 716.92 1.794 38 714.97 1.789 42 713.38 1.786 46 711.55 1.781 42 710.08 1.777 45 707.89 1.772 45 706.42 1.768 42 704.47 1.763 44 702.88 1.759 43 701.05 1.755 42 699.95 1.752 41 693.73 1.736 76 690.19 1.727 86 686.52 1.718 119 685.18 1.715 119 677.98 1.697 97 675.54 1.691 132 672.49 1.683 124 668.95 1.674 72 640.38 1.603 51 636.60 1.593 41 631.10 1.580 36 628.78 1.574 40 627.20 1.570 37 378.05 0.946 35 377.81 0.946 35 375.85 0.941 38 366.94 0.919 35
liquid film
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