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Iodoethane

Product Name Iodoethane

CAS75-03-6

MFC2H5I

MW155.97

¹³CNMR

Mass

MS-NW-0530          
iodoethane
C2H5I               (Mass of molecular ion:    156)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      26.0       7.1
      27.0      57.5
      28.0       7.4
      29.0      99.9
      30.0       2.4
     127.0      16.8
     128.0       5.4
     141.0       1.8
     156.0     100.0
     157.0       2.2

90 MHz in CDCl3

parameter in CDCl3

¹H NMR	89.56 MHz
C₂ H₅ I	0.04 ml : 0.5 ml CDCl₃
iodoethane

    Assign.     Shift(ppm)

      A             3.186
      B             1.847
     
     J(A,B)=7.6HZ

     Hz     ppm     Int.

    297.69   3.324     92
    297.00   3.317     93
    289.81   3.236    341
    282.94   3.160    221
    282.31   3.153    404
    275.31   3.075    133
    274.69   3.068    127
    172.38   1.925    406
    165.19   1.845   1000
    164.75   1.840    593
    157.50   1.759    311

¹H NMR	300 MHz
C₂ H₅ I	10 vol% in CCl₄
iodoethane

    Parameter     ppm  Hz

      D(A)         1.859
      D(B)         3.155
       J(A,B)          7.446
     
     EBERSOLE,S. ET AL. J.PHYS.CHEM. 68, 3430 (1964)

     Hz     ppm     Int.

    957.78   3.193    152
    950.32   3.168    472
    942.88   3.143    489
    935.45   3.118    170
    565.08   1.884    509
    557.64   1.859   1000
    550.19   1.834    467

in CDCl3

CCl4 solution

liquid film

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