3,5-DINITROBENZYL CHLORIDE

Mass

MS-NW-7259          
3,5-dinitrobenzyl chloride
C7H5ClN2O4          (Mass of molecular ion:    216)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      28.0       2.1
      30.0      24.5
      37.0       1.5
      38.0       3.2
      39.0      12.3
      46.0       1.0
      49.0       1.7
      50.0       4.8
      51.0       7.7
      52.0       1.6
      61.0       2.4
      62.0      10.5
      63.0      26.9
      64.0       2.5
      65.0       1.5
      73.0       4.5
      74.0       2.6
      75.0      10.0
      76.0       2.4
      77.0       8.3
      78.0       1.1
      85.0       1.7
      86.0       3.1
      87.0       4.6
      88.0       4.2
      89.0      32.0
      90.0       2.8
      97.0       1.2
     105.0      11.2
     106.0       1.1
     112.0       1.3
     123.0      27.0
     124.0      17.3
     125.0      10.2
     126.0       6.0
     134.0       1.0
     135.0       6.5
     140.0       6.4
     142.0       2.2
     169.0       2.5
     170.0      12.6
     171.0       1.8
     172.0       4.2
     181.0     100.0
     182.0       8.8
     183.0       1.2
     199.0       4.4
     200.0       1.2
     201.0       1.6
     216.0      47.1
     217.0       4.3
     218.0      16.1
     219.0       1.4

Assign. Shift(ppm) A 9.003 B 8.622 C 4.785 J(A,B)=2.1HZ J(B,C)=1.0HZ

     Hz     ppm     Int.

    810.88   9.055     27
    810.50   9.050     30
    808.50   9.028    166
    806.44   9.005    310
    804.38   8.982    186
    802.56   8.962     27
    777.31   8.680     36
    773.06   8.632    672
    771.00   8.609    584
    428.81   4.788   1000
    428.38   4.784    932