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4457-32-3

4-Nitrobenzyl chloroformate

Product Name 4-Nitrobenzyl chloroformate

CAS4457-32-3

MFC8H6ClNO4

MW215.59

  • 4457-32-3_ms_1
    Mass

    MS-NW-7976          
    p-nitrobenzyl chloroformate
    C8H6ClNO4           (Mass of molecular ion:    215)
    

       Source Temperature: 150 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          18.0       1.4
          27.0       3.1
          28.0       4.2
          29.0       3.1
          30.0      52.0
          36.0       1.6
          37.0       1.4
          38.0       3.9
          39.0      12.2
          40.0       2.1
          44.0       4.5
          50.0       9.7
          51.0      16.2
          52.0       4.6
          61.0       1.1
          62.0       4.2
          63.0      18.4
          64.0       6.1
          65.0       5.7
          66.0       1.0
          74.0       2.4
          75.0       3.9
          76.0       5.0
          77.0      15.9
          78.0      25.9
          79.0       2.2
          89.0      77.1
          90.0      20.2
          91.0       1.6
          92.0       1.1
          94.0       1.0
          99.0       2.3
         104.0       1.5
         105.0       3.7
         106.0      17.8
         107.0       1.8
         113.0       1.4
         124.0       1.8
         125.0       9.2
         126.0       1.2
         127.0       3.2
         135.0      11.9
         136.0     100.0
         137.0       8.3
         141.0       3.3
         143.0       1.3
         152.0       4.4
         154.0       2.2
         169.0       2.2
         171.0       7.1
         173.0       2.1
         179.0       1.1
         199.0       3.1
         215.0      33.7
         216.0       4.7
         217.0      11.1
         218.0       1.6
    

400 MHz in CDCl3

  • 4457-32-3_1hnmr_1

    1H NMR 399.65 MHz
    C8 H6 Cl N O4 0.05 ml : 0.5 ml CDCl3
    p-nitrobenzyl chloroformate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.255 B 7.601 C 5.430

         Hz     ppm     Int.
    

       3306.27   8.273     91
       3303.96   8.268    527
       3302.00   8.263    203
       3297.12   8.251    191
       3295.17   8.246    572
       3292.97   8.240    104
       3044.80   7.619     96
       3042.48   7.613    471
       3040.41   7.608    204
       3035.64   7.596    220
       3033.57   7.591    501
       3031.25   7.585    134
       2170.41   5.431   1000
    

in CDCl3

  • 4457-32-3_13cnmr_1

KBr disc

  • 4457-32-3_ir1_2

nujol mull

  • 4457-32-3_ir2_1

  • 4457-32-3_raman