PYRIDINE-2-CARBOXALDEHYDE 2-QUINOLYLHYDRAZONE

Mass

MS-NW-6899          
2-pyridinecarbaldehyde 2-quinolylhydrazone
C15H12N4            (Mass of molecular ion:    248)

   Source Temperature: 200 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       3.3
      27.0       1.1
      28.0       1.1
      38.0       1.0
      39.0       3.3
      50.0       1.6
      51.0       4.5
      52.0       2.5
      62.0       1.0
      63.0       2.7
      64.0       2.0
      65.0       9.2
      75.0       1.9
      76.0       1.4
      77.0       2.4
      78.0       3.1
      79.0       2.3
      88.0       1.1
      89.0       3.8
      90.0       2.1
      91.0       1.4
      92.0       5.5
     101.0       2.9
     102.0       2.4
     105.0       1.4
     114.0       1.0
     115.0       2.5
     116.0       5.7
     117.0       5.0
     128.0       5.3
     129.0       2.9
     142.0       1.5
     143.0       3.2
     144.0      10.6
     145.0       1.3
     169.0       1.1
     170.0     100.0
     171.0      13.0
     218.0       1.4
     219.0       5.1
     220.0       1.7
     245.0       5.0
     246.0       2.6
     247.0       1.7
     248.0      14.8
     249.0       3.0

Assign. Shift(ppm) A 11.5 B 8.578 C 8.217 D 8.203 E 8.037 F 7.834 G 7.81 J 7.696 K 7.684 L 7.619 M 7.32

     Hz     ppm     Int.

   4605.90  11.525    320
   3431.81   8.588    236
   3431.07   8.586    280
   3430.34   8.584    281
   3429.43   8.582    240
   3427.05   8.576    250
   3426.13   8.573    288
   3425.58   8.572    275
   3424.66   8.570    222
   3289.49   8.231    401
   3280.33   8.209    544
   3278.31   8.203   1000
   3216.59   8.049    336
   3208.53   8.029    410
   3139.11   7.855    161
   3137.64   7.851    160
   3131.60   7.836    283
   3129.95   7.832    277
   3123.72   7.817    419
   3116.39   7.798    313
   3080.31   7.708    632
   3076.28   7.698    254
   3071.34   7.686    621
   3068.04   7.677    444
   3052.29   7.638    223
   3051.00   7.635    215
   3045.51   7.621    258
   3044.04   7.617    315
   3042.58   7.614    142
   3037.08   7.600    150
   3035.80   7.597    135
   2936.71   7.349    210
   2935.43   7.346    212
   2932.13   7.337    244
   2931.03   7.334    267
   2928.65   7.329    401
   2927.55   7.326    413
   2926.45   7.323    278
   2924.80   7.319    248
   2923.70   7.316    228
   2921.87   7.312    213
   2920.22   7.307    289
   2918.94   7.304    205