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MS-IW-2341 2-hydrazinopyridine C5H7N3 (Mass of molecular ion: 109)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 1.9 27.0 3.3 28.0 10.2 29.0 1.0 31.0 1.6 37.0 1.9 38.0 4.7 39.0 10.3 40.0 3.2 41.0 3.0 44.0 1.9 49.0 1.0 50.0 5.5 51.0 13.8 52.0 30.8 53.0 10.3 54.0 1.2 54.5 1.0 64.0 2.6 65.0 5.6 66.0 7.0 67.0 10.4 78.0 11.2 79.0 82.9 80.0 12.4 81.0 1.1 92.0 2.0 93.0 2.2 94.0 9.7 108.0 8.1 109.0 100.0 110.0 6.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H7 N3 0.039 g : 0.5 ml CDCl3 2-hydrazinopyridine Assign. Shift(ppm)
A 8.11 B 7.450 C 6.68 D 6.65 E 3.8
Hz ppm Int.
729.19 8.142 175 724.25 8.087 185 719.69 8.036 33 676.75 7.557 438 674.88 7.536 423 669.75 7.479 505 668.19 7.461 603 667.81 7.457 524 666.38 7.441 497 661.25 7.384 673 659.38 7.363 616 603.63 6.740 186 602.63 6.729 768 601.31 6.715 768 600.25 6.703 212 598.44 6.683 30 596.44 6.660 455 595.38 6.648 405 594.25 6.636 1000 593.19 6.624 365 589.38 6.581 334 588.31 6.569 270 340.88 3.807 78
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