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Trimethyl orthobenzoate

Product Name Trimethyl orthobenzoate

CAS707-07-3

MFC10H14O3

MW182.22

¹³CNMR

Mass

MS-NW-6423          
trimethyl orthobenzoate
C10H14O3            (Mass of molecular ion:    182)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       6.4
      29.0       1.9
      31.0       1.2
      39.0       1.2
      45.0       2.0
      50.0       3.5
      51.0       9.4
      59.0      10.5
      65.0       1.4
      74.0       1.0
      75.0       1.1
      76.0       1.4
      77.0      23.9
      78.0       2.1
      79.0       1.3
      91.0      11.3
      92.0       3.3
     105.0      47.0
     106.0       3.8
     136.0       3.6
     151.0     100.0
     152.0      10.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₄ O₃	0.05 ml : 0.5 ml CDCl₃
trimethyl orthobenzoate

    Assign.     Shift(ppm)

      A             7.55
      B          7.42 to 7.29
      C             3.128

     Hz     ppm     Int.

    683.88   7.637     20
    679.94   7.593     34
    678.94   7.581     25
    676.38   7.553     46
    674.00   7.526     55
    664.38   7.419     31
    663.50   7.409     26
    661.94   7.392     66
    660.81   7.379     56
    657.56   7.343     64
    654.88   7.313     58
    280.25   3.130   1000

in CDCl3

liquid film

4880 A,200 M,liquid

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