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MS-IW-8602 1-chloro-3-iodopropane C3H6ClI (Mass of molecular ion: 204)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.1 26.0 1.5 27.0 13.3 28.0 2.9 36.0 1.3 37.0 1.4 38.0 2.8 39.0 21.0 40.0 3.1 41.0 89.8 42.0 5.4 49.0 16.1 51.0 5.4 61.0 1.7 75.0 2.4 76.0 3.0 77.0 100.0 78.0 4.4 79.0 33.7 80.0 1.1 127.0 11.8 128.0 4.2 141.0 5.5 155.0 6.0 169.0 3.6 204.0 57.7 205.0 1.9 206.0 18.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H6 Cl I 0.05 ml : 0.5 ml CDCl3 1-chloro-3-iodopropane Assign. Shift(ppm)
A 3.644 B 3.334 C 2.230
Hz ppm Int.
1462.65 3.660 593 1460.69 3.655 58 1456.54 3.645 916 1450.44 3.630 602 1447.39 3.622 29 1338.99 3.351 599 1332.40 3.334 1000 1329.59 3.327 47 1325.93 3.318 598 903.56 2.261 186 897.22 2.246 486 895.14 2.240 52 894.53 2.239 52 890.99 2.230 601 884.77 2.214 454 878.30 2.198 164
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