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MassMS-NW-8866 5-methylene-2-norbornene C8H10 (Mass of molecular ion: 106)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 8.3 38.0 2.6 39.0 21.1 40.0 6.7 41.0 5.1 50.0 4.6 51.0 11.6 52.0 5.4 53.0 4.1 62.0 1.6 63.0 4.5 64.0 1.0 65.0 14.1 66.0 100.0 67.0 7.6 74.0 1.0 77.0 16.3 78.0 44.3 79.0 17.6 80.0 3.2 89.0 1.1 91.0 77.7 92.0 6.6 93.0 1.2 103.0 4.6 104.0 1.3 105.0 18.4 106.0 31.5 107.0 2.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 0.05 ml : 0.5 ml CDCl3 5-methylene-2-norbornene 
Assign. Shift(ppm)
A *1 6.108 B *1 6.060 C *2 4.979 D *2 4.705 E 3.139 F 2.949 G *3 2.244 J *3 1.746 K *4 1.587 L *4 1.410
Hz ppm Int.2446.17 6.121 518 2443.24 6.114 532 2440.55 6.107 827 2437.62 6.100 842 2425.90 6.071 647 2425.17 6.069 667 2422.85 6.063 632 2422.12 6.061 649 2421.26 6.059 412 2420.29 6.057 412 2419.68 6.055 388 2417.24 6.049 387 2416.50 6.047 374 1989.87 4.980 904 1881.23 4.708 1000 1880.74 4.706 938 1879.88 4.704 935 1879.52 4.703 1000 1256.59 3.145 586 1255.49 3.142 683 1255.00 3.141 688 1254.39 3.139 689 1254.03 3.138 681 1252.93 3.136 584 1179.93 2.953 570 1179.44 2.952 575 1178.96 2.950 576 1178.47 2.949 574 903.93 2.262 362 903.32 2.261 323 902.22 2.258 419 900.51 2.254 358 889.77 2.227 329 889.28 2.226 413 888.67 2.224 367 888.18 2.223 348 887.45 2.221 488 886.72 2.219 345 886.23 2.218 348 885.74 2.217 402 706.67 1.769 380 706.30 1.768 384 705.20 1.765 381 703.49 1.761 398 691.65 1.731 329 690.43 1.728 326 688.84 1.724 345 640.26 1.603 389 638.67 1.599 388 637.08 1.595 363 632.08 1.582 470 630.49 1.578 473 628.91 1.574 438 567.38 1.420 729 559.20 1.400 600
in CDCl3
liquid film
4880 A,150M,liquid
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