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MS-NW-3601 norbornylene C7H10 (Mass of molecular ion: 94)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 4.9 38.0 1.5 39.0 10.6 40.0 4.4 41.0 3.3 50.0 1.4 51.0 2.8 52.0 1.1 53.0 2.5 63.0 1.3 65.0 5.8 66.0 100.0 67.0 6.7 77.0 6.5 78.0 1.4 79.0 10.4 91.0 3.1 93.0 1.7 94.0 8.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H10 0.038 g : 0.5 ml CDCl3 norbornylene Assign. Shift(ppm)
A 5.989 B 2.844 C *1 1.61 D *2 1.313 E *2 1.076 F *1 0.95
Hz ppm Int.
2395.51 5.995 637 2393.80 5.990 1000 2392.09 5.986 647 1142.09 2.858 119 1140.38 2.854 300 1138.67 2.850 552 1136.96 2.845 673 1135.25 2.841 567 1133.42 2.837 319 1131.71 2.832 128 651.49 1.631 126 649.17 1.625 214 647.46 1.621 325 646.00 1.617 365 645.39 1.615 422 643.92 1.612 311 642.94 1.609 179 640.99 1.604 177 640.14 1.602 309 638.79 1.599 460 637.82 1.596 372 636.60 1.593 370 635.01 1.589 250 632.69 1.584 137 531.37 1.330 149 529.30 1.325 222 527.22 1.320 161 525.39 1.315 117 523.32 1.310 179 521.36 1.305 256 519.29 1.300 182 433.72 1.086 322 432.37 1.082 200 427.25 1.070 157 425.78 1.066 274 424.32 1.062 169 389.40 0.975 166 387.08 0.969 191 385.50 0.965 498 383.06 0.959 464 379.03 0.949 232 378.05 0.946 460 376.71 0.943 256 375.73 0.941 468 374.02 0.936 183 371.58 0.930 149
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