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1-Methylcyclopentene

Product Name 1-Methylcyclopentene

CAS693-89-0

MFC6H10

MW82.14

¹³CNMR

Mass

MS-NW-3064          
1-methyl-1-cyclopentene
C6H10               (Mass of molecular ion:     82)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       1.0
      27.0       7.3
      29.0       1.5
      38.0       1.7
      39.0      13.5
      40.0       2.7
      41.0      16.0
      42.0       2.2
      43.0       1.2
      50.0       2.6
      51.0       3.8
      52.0       1.8
      53.0       8.2
      54.0       6.1
      55.0       2.8
      65.0       4.6
      66.0       2.1
      67.0     100.0
      68.0       5.6
      77.0       3.1
      79.0       8.1
      80.0       2.1
      81.0      18.1
      82.0      31.3
      83.0       2.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₀	0.04 ml : 0.5 ml CDCl₃
1-methyl-1-cyclopentene

    Assign.     Shift(ppm)

      A             5.30
      B          2.36 to 2.11
      C             1.90
      D             1.72

     Hz     ppm     Int.

    477.38   5.331    145
    477.06   5.327    175
    476.63   5.322    134
    475.56   5.310    256
    475.25   5.307    246
    473.75   5.290    280
    472.13   5.272    179
    470.81   5.257     63
    470.38   5.253     63
    470.06   5.249     60
    469.75   5.246     64
    216.50   2.418     35
    216.06   2.413     40
    215.38   2.405     41
    214.31   2.393     70
    214.00   2.390     65
    213.25   2.382     74
    212.75   2.376     59
    212.19   2.370     83
    211.81   2.366     89
    211.19   2.359     78
    210.56   2.352    112
    209.69   2.342    141
    209.13   2.336    156
    208.75   2.331    178
    207.63   2.319    233
    206.69   2.308    232
    205.56   2.296    268
    204.31   2.282    267
    203.50   2.273    298
    202.69   2.264    262
    201.94   2.255    436
    201.38   2.249    389
    200.63   2.241    308
    199.38   2.227    379
    198.25   2.214    337
    197.69   2.208    302
    196.63   2.196    455
    195.69   2.186    339
    194.75   2.175    384
    194.13   2.168    334
    193.50   2.161    267
    193.06   2.156    231
    192.38   2.149    237
    191.56   2.139    265
    190.63   2.129    171
    189.94   2.121    146
    189.06   2.111    120
    188.56   2.106     96
    188.13   2.101     69
    187.06   2.089     65
    186.06   2.078     56
    185.25   2.069     38
    184.38   2.059     34
    182.50   2.038     65
    181.25   2.024    104
    180.81   2.019     62
    179.94   2.010    148
    179.63   2.006    152
    178.69   1.996    100
    178.00   1.988    280
    177.06   1.977     58
    176.50   1.971     65
    175.81   1.964     56
    174.13   1.945    254
    173.44   1.937    166
    173.13   1.934    171
    172.06   1.922    371
    170.31   1.902     71
    169.56   1.894     84
    168.38   1.881    123
    167.94   1.876    173
    165.94   1.853    270
    165.19   1.845    334
    164.50   1.837    171
    163.31   1.824    113
    162.81   1.818    106
    161.81   1.807    106
    161.06   1.799     72
    160.56   1.793     87
    160.19   1.789     81
    158.63   1.772    211
    157.75   1.762    218
    156.75   1.751    384
    155.75   1.740    674
    155.19   1.733    725
    154.69   1.728   1000
    154.19   1.722    821
    153.69   1.717    710
    153.13   1.710    923
    152.06   1.698    694
    151.06   1.687    469
    149.94   1.675    241
    149.25   1.667    113
    147.56   1.648     41

in CDCl3

liquid film

4880 A,200 M,liquid

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