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6602-28-4

3-Pyridinol N-oxide

Product Name 3-Pyridinol N-oxide

CAS6602-28-4

MFC5H5NO2

MW111.1

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  • 6602-28-4_ms
    Mass

    MS-NW-1994          
    3-pyridinol N-oxide
    C5H5NO2             (Mass of molecular ion:    111)
    

       Source Temperature: 170 °C
       Sample Temperature: 200 °C
       Direct, 75 eV
    

          14.0       1.5
          17.0       3.9
          18.0      19.7
          20.0       1.7
          25.0       1.5
          26.0       9.3
          27.0      15.7
          28.0      21.3
          29.0       8.5
          30.0       3.8
          32.5       1.1
          36.0       1.0
          37.0       7.4
          38.0      16.5
          39.0      46.1
          40.0      18.3
          41.0      16.9
          42.0       7.4
          43.0       3.0
          44.0       8.2
          45.0       1.4
          49.0       1.8
          50.0       5.7
          51.0       6.8
          52.0       4.9
          53.0       5.1
          54.0       8.8
          55.0      39.3
          55.5       1.0
          56.0       7.0
          57.0       2.2
          58.0       2.4
          62.0       1.2
          63.0       1.8
          64.0       1.5
          65.0       2.3
          66.0       7.2
          67.0      13.5
          68.0      14.3
          69.0       1.9
          71.0       1.4
          76.0       1.3
          77.0       1.2
          81.0       1.3
          82.0       5.4
          83.0       1.3
          84.0       7.4
          94.0       6.6
          95.0     100.0
          96.0       6.1
         106.0       1.1
         109.0       1.4
         111.0      91.9
         112.0       5.6
    

400 MHz in DMSO-d6

  • 6602-28-4_1hnmr

    1H NMR 399.65 MHz
    C5 H5 N O2 0.038 g : 0.5 ml DMSO-d6
    3-pyridinol N-oxide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.8 B 7.824 C 7.802 D 7.257 E 6.878

         Hz     ppm     Int.
    

       4319.80  10.809    116
       3129.03   7.830    517
       3127.20   7.825   1000
       3125.37   7.821    758
       3122.44   7.813    538
       3121.71   7.812    589
       3120.79   7.809    402
       3120.06   7.807    333
       3116.21   7.798    537
       3115.48   7.796    542
       3114.56   7.794    456
       3113.83   7.792    388
       2907.95   7.277    460
       2905.20   7.270     36
       2904.65   7.268     38
       2901.72   7.261    463
       2899.53   7.256    525
       2896.05   7.247     37
       2893.30   7.240    478
       2754.46   6.893    457
       2753.54   6.890    476
       2752.26   6.887    471
       2751.53   6.885    441
       2745.85   6.871    421
       2745.12   6.869    420
       2743.65   6.866    431
       2742.92   6.864    394
    

in DMSO-d6

  • 6602-28-4_13cnmr

KBr disc

  • 6602-28-4_ir1_2

nujol mull

  • 6602-28-4_ir2_1

  • 6602-28-4_raman