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3,5-Dichlorobenzonitrile

Product Name 3,5-Dichlorobenzonitrile

CAS6575-00-4

MFC7H3Cl2N

MW172.01

¹³CNMR

Mass

MS-NW-6528          
3,5-dichlorobenzonitrile
C7H3Cl2N            (Mass of molecular ion:    171)

   Source Temperature: 240 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      36.0       1.0
      37.0       2.9
      38.0       1.6
      49.0       2.4
      50.0      10.4
      50.5       1.1
      51.0       1.4
      60.0       1.4
      61.0       1.8
      62.0       1.5
      67.5       1.4
      72.0       1.7
      73.0       3.4
      74.0       5.3
      75.0       6.8
      76.0       2.5
      84.0       2.6
      85.0       2.4
      85.5       3.5
      86.0       1.8
      86.5       2.1
      87.0       1.1
      99.0       4.0
     100.0      15.9
     101.0       2.1
     109.0       2.8
     110.0       2.4
     111.0       1.4
     135.0       2.5
     136.0      18.4
     137.0       2.2
     138.0       6.1
     171.0     100.0
     172.0       8.4
     173.0      64.3
     174.0       5.2
     175.0      10.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₃ Cl₂ N	0.040 g : 0.5 ml CDCl₃
3,5-dichlorobenzonitrile

    Assign.     Shift(ppm)

      A             7.602
      B             7.548
     
     CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

    683.25   7.629    117
    681.75   7.613    175
    681.06   7.605    247
    679.56   7.588    435
    676.75   7.557   1000
    675.06   7.538    416
    674.56   7.532    304

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

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