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MS-NW-9583 2-methyl-6-quinolinamine C10H10N2 (Mass of molecular ion: 158)
Source Temperature: 170 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 1.6 28.0 1.1 51.0 1.6 52.0 1.3 63.0 1.6 64.5 1.1 65.0 2.3 66.0 1.6 77.0 2.7 78.0 2.2 79.0 5.3 89.0 2.4 102.0 1.0 103.0 3.6 104.0 1.5 115.0 1.0 116.0 2.5 117.0 1.0 128.0 1.1 130.0 11.3 131.0 4.5 132.0 1.1 140.0 1.5 141.0 1.1 142.0 4.1 143.0 2.4 155.0 1.9 156.0 2.0 157.0 26.6 158.0 100.0 159.0 12.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H10 N2 0.032 g : 0.5 ml CDCl3 2-methyl-6-quinolinamine Assign. Shift(ppm)
A *1 7.82 B *1 7.78 C 7.148 D 7.102 E 6.856 F 3.9 G 2.662
Hz ppm Int.
705.38 7.877 107 701.25 7.830 101 696.38 7.776 137 693.13 7.740 125 643.81 7.189 187 641.75 7.166 109 639.25 7.138 118 635.44 7.096 140 632.94 7.068 82 630.25 7.038 103 615.13 6.869 153 612.56 6.840 125 351.63 3.927 39 350.25 3.911 40 349.94 3.908 41 349.06 3.898 45 348.75 3.895 43 348.25 3.889 46 347.94 3.885 47 347.19 3.877 47 346.19 3.866 49 345.31 3.856 45 344.50 3.847 45 343.88 3.840 43 343.44 3.835 40 342.75 3.828 38 342.38 3.823 38 238.44 2.663 1000
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