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1-(4-Fluorophenyl)piperazine dihydrochloride

Product Name 1-(4-Fluorophenyl)piperazine dihydrochloride

CAS64090-19-3

MFC10H15Cl2FN2

MW253.14

¹³CNMR

Mass

MS-IW-2169          
1-(p-fluorophenyl)piperazine dihydrochloride
C10H13FN2 2HCl      (Mass of molecular ion:    180)

   Source Temperature: 150 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      18.0       1.0
      28.0       3.2
      29.0       2.9
      30.0       1.9
      35.0       1.7
      36.0      17.9
      38.0       6.0
      42.0       1.7
      56.0       6.7
      57.0       4.1
      75.0       2.8
      90.0       1.5
      95.0       7.9
      96.0       1.4
     109.0       4.1
     122.0      10.0
     123.0      11.1
     124.0       4.5
     125.0       1.0
     138.0     100.0
     139.0       9.2
     150.0       1.1
     180.0      35.8
     181.0       4.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₃ F N₂	0.032 g : 0.5 ml DMSO-d₆
1-(p-fluorophenyl)piperazine dihydrochloride

    Assign.     Shift(ppm)

      A             9.78
      B             7.170
      C             6.56
      D             3.451
      E             3.273

     Hz     ppm     Int.

   3908.54   9.780     70
   2868.96   7.179   1000
   2862.40   7.163    963
   2620.24   6.557    194
   1384.74   3.465    215
   1379.85   3.453    311
   1374.36   3.439    282
   1308.29   3.274    232

in DMSO-d6

KBr disc

nujol mull

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